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Characterization and modeling of microstructural stresses in alumina

Journal of the American Ceramic Society

Teague, Melissa C.; Rodgers, Theron R.; Grutzik, Scott J.; Meserole, Stephen M.

Brittle failure is often influenced by difficult to measure and variable microstructure-scale stresses. Recent advances in photoluminescence spectroscopy (PLS), including improved confocal laser measurement and rapid spectroscopic data collection have established the potential to map stresses with microscale spatial resolution (< 2 μm). Advanced PLS was successfully used to investigate both residual and externally applied stresses in polycrystalline alumina at the microstructure scale. The measured average stresses matched those estimated from beam theory to within one standard deviation, validating the technique. Modeling the residual stresses within the microstructure produced qualitative agreement in comparison with the experimentally measured results. Microstructure scale modeling is primed to take advantage of advanced PLS to enable its refinement and validation, eventually enabling microstructure modeling to become a predictive tool for brittle materials.

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Designing brittle fracture specimens to investigate environmentally assisted crack growth

Conference Proceedings of the Society for Experimental Mechanics Series

Aduloju, Sunday; Gu, Wenjia; Truster, Timothy; Emery, John M.; Reedy, Earl D.; Grutzik, Scott J.

Subcritical crack growth can occur in a glass when the stress intensity factor is less than the fracture toughness if water molecules are present. A novel bi-material beam specimen is proposed to investigate environmentally assisted crack growth (EACG). Two materials with different coefficients of thermal expansion are diffusion bonded at high temperature and cooled to the room temperature which introduces residual stress in the beam. A Finite element (FE) model is developed and initially validated with an analytical model. Steady-state crack (SSC) depth at which mode II stress intensity factor (KII) is zero and the corresponding mode I stress intensity factor (KI) value are obtained for different material pairs and thickness ratios of the top and bottom materials using the FE model. Crack propagation path is also predicted. We finally modify the geometry of the specimen to generate non-constant KI values as the crack propagates.

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Crack Path Selection in Thermally Loaded Borosilicate/Steel Bibeam Specimen

Experimental Mechanics

Grutzik, Scott J.; Reedy, Earl D.

We have developed a novel specimen for studying crack paths in glass. Under certain conditions, the specimen reaches a state where the crack must select between multiple paths satisfying the KII = 0 condition. This path selection is a simple but challenging benchmark case for both analytical and numerical methods of predicting crack propagation. We document the development of the specimen, using an uncracked and instrumented test case to study the effect of adhesive choice and validate the accuracy of both a simple beam theory model and a finite element model. In addition, we present preliminary fracture test results and provide a comparison to the path predicted by two numerical methods (mesh restructuring and XFEM). The directional stability of the crack path and differences in kink angle predicted by various crack kinking criteria is analyzed with a finite element model.

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Microstructural Modeling of Brittle Materials for Enhanced Performance and Reliability

Teague, Melissa C.; Teague, Melissa C.; Rodgers, Theron R.; Rodgers, Theron R.; Grutzik, Scott J.; Grutzik, Scott J.; Meserole, Stephen M.; Meserole, Stephen M.

Brittle failure is often influenced by difficult to measure and variable microstructure-scale stresses. Recent advances in photoluminescence spectroscopy (PLS), including improved confocal laser measurement and rapid spectroscopic data collection have established the potential to map stresses with microscale spatial resolution (%3C2 microns). Advanced PLS was successfully used to investigate both residual and externally applied stresses in polycrystalline alumina at the microstructure scale. The measured average stresses matched those estimated from beam theory to within one standard deviation, validating the technique. Modeling the residual stresses within the microstructure produced general agreement in comparison with the experimentally measured results. Microstructure scale modeling is primed to take advantage of advanced PLS to enable its refinement and validation, eventually enabling microstructure modeling to become a predictive tool for brittle materials.

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Development of glass/steel bibeam specimen for study of brittle crack path stability

Conference Proceedings of the Society for Experimental Mechanics Series

Grutzik, Scott J.; Reedy, Earl D.

We have developed a novel specimen for studying crack paths in glass. Under certain conditions, the specimen reaches a state where the crack must select between multiple paths satisfying the Kπ 0 condition. This path selection is a simple but difficult benchmark case for both analytical and numerical methods of predicting crack propagation. We document the development of the specimen, using an uncracked and instrumented test case to study the effect of adhesive choice and validate the accuracy of both a simple beam theory model and a finite element model. In addition, we present preliminary fracture test results and provide a comparison to the path predicted by two numerical methods (mesh restructuring and XFEM).

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Results 26–50 of 54
Results 26–50 of 54