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Nanoindentation and TEM Characterization of Ion Irridiated 316L Stainless Steels

Energy Technology 2012: Carbon Dioxide Management and Other Technologies

Hattar, Khalid M.; Buchheit, Thomas E.; Kotula, Paul G.; Mcginnis, Alexander; Brewer, Luke

Understanding the effects of extensive radiation damage in structural metals provides necessary insight for predicting the performance of those metals considered for application in the extreme radiation environment. Predicting mechanical performance after long term radiation exposure is of great importance to extending the life of current nuclear reactors and for developing future materials for the next generation of reactors. A combination of finite element modeling, nanoindentation, and TEM characterization were used to rapidly determine the microstructure and mechanical properties influences of ion irradiation on a standard 316L stainless steel sample. The results of this study found that ion irradiation and small scale mechanical property testing can be used to characterize extensive levels of radiation damage structure, only when significant consideration is given to ion irradiation depth, surface roughness and polishing condition, the irradiation temperature, and.many other experimental parameters. © 2012 The Minerals, Metals, & Materials Society. All rights reserved.

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TYPE Conference YEAR 2012
ScopusOSTI

Fast neutron environments

Hattar, Khalid M.; Puskar, J.D.; Doyle, Barney L.; Boyce, Brad B.; Buchheit, Thomas E.; Foiles, Stephen M.; Lu, Ping L.; Clark, Blythe C.; Kotula, Paul G.; Goods, Steven H.

The goal of this LDRD project is to develop a rapid first-order experimental procedure for the testing of advanced cladding materials that may be considered for generation IV nuclear reactors. In order to investigate this, a technique was developed to expose the coupons of potential materials to high displacement damage at elevated temperatures to simulate the neutron environment expected in Generation IV reactors. This was completed through a high temperature high-energy heavy-ion implantation. The mechanical properties of the ion irradiated region were tested by either micropillar compression or nanoindentation to determine the local properties, as a function of the implantation dose and exposure temperature. In order to directly compare the microstructural evolution and property degradation from the accelerated testing and classical neutron testing, 316L, 409, and 420 stainless steels were tested. In addition, two sets of diffusion couples from 316L and HT9 stainless steels with various refractory metals. This study has shown that if the ion irradiation size scale is taken into consideration when developing and analyzing the mechanical property data, significant insight into the structural properties of the potential cladding materials can be gained in about a week.

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TYPE SAND Report YEAR 2011
OSTIDOI
Results 451–500 of 527
Results 451–500 of 527