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Automated high-throughput tensile testing reveals stochastic process parameter sensitivity

Materials Science and Engineering: A

Heckman, Nathan H.; Ivanoff, Thomas I.; Roach, Ashley M.; Jared, Bradley H.; Tung, Daniel J.; Brown-Shaklee, Harlan J.; Huber, Todd H.; Saiz, David J.; Koepke, Joshua R.; Rodelas, Jeffrey R.; Madison, Jonathan D.; Salzbrenner, Bradley S.; Swiler, Laura P.; Jones, Reese E.; Boyce, Brad B.

The mechanical properties of additively manufactured metals tend to show high variability, due largely to the stochastic nature of defect formation during the printing process. This study seeks to understand how automated high throughput testing can be utilized to understand the variable nature of additively manufactured metals at different print conditions, and to allow for statistically meaningful analysis. This is demonstrated by analyzing how different processing parameters, including laser power, scan velocity, and scan pattern, influence the tensile behavior of additively manufactured stainless steel 316L utilizing a newly developed automated test methodology. Microstructural characterization through computed tomography and electron backscatter diffraction is used to understand some of the observed trends in mechanical behavior. Specifically, grain size and morphology are shown to depend on processing parameters and influence the observed mechanical behavior. In the current study, laser-powder bed fusion, also known as selective laser melting or direct metal laser sintering, is shown to produce 316L over a wide processing range without substantial detrimental effect on the tensile properties. Ultimate tensile strengths above 600 MPa, which are greater than that for typical wrought annealed 316L with similar grain sizes, and elongations to failure greater than 40% were observed. It is demonstrated that this process has little sensitivity to minor intentional or unintentional variations in laser velocity and power.

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TYPE Journal Article YEAR 2020
ScopusOSTIDOI

Linking pyrometry to porosity in additively manufactured metals

Additive Manufacturing

Mitchell, John A.; Ivanoff, Thomas I.; Dagel, Daryl; Madison, Jonathan D.; Jared, Bradley H.

Porosity in additively manufactured metals can reduce material strength and is generally undesirable. Although studies have shown relationships between process parameters and porosity, monitoring strategies for defect detection and pore formation are still needed. In this paper, instantaneous anomalous conditions are detected in-situ via pyrometry during laser powder bed fusion additive manufacturing and correlated with voids observed using post-build micro-computed tomography. Large two-color pyrometry data sets were used to estimate instantaneous temperatures, melt pool orientations and aspect ratios. Machine learning algorithms were then applied to processed pyrometry data to detect outlier images and conditions. It is shown that melt pool outliers are good predictors of voids observed post-build. With this approach, real time process monitoring can be incorporated into systems to detect defect and void formation. Alternatively, using the methodology presented here, pyrometry data can be post processed for porosity assessment.

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TYPE Journal Article YEAR 2020
ScopusOSTIDOI

Evolution of damage and failure in an additively manufactured 316L SS structure: experimental reinvestigation of the third Sandia fracture challenge

International Journal of Fracture

Kramer, S.L.B.; Ivanoff, Thomas I.; Madison, Jonathan D.; Lentfer, Andrew L.

The third Sandia Fracture Challenge (SFC3) was a benchmark problem for comparing experimental and simulated ductile deformation and failure in an additively manufactured (AM) 316L stainless steel structure. One surprising observation from the SFC3 was the Challenge-geometry specimens had low variability in global load versus displacement behavior, attributed to the large stress-concentrating geometric features dominating the global behavior, rather than the AM voids that tend to significantly influence geometries with uniform cross-sections. This current study reinvestigates the damage and failure evolution of the Challenge-geometry specimens, utilizing interrupted tensile testing with micro-computed tomography (micro-CT) scans to monitor AM void and crack growth from a virgin state through complete failure. This study did not find a correlation between global load versus displacement behavior and AM void attributes, such as void volume, location, quantity, and relative size, which incidentally corroborates the observation from the SFC3. However, this study does show that the voids affect the local behavior of damage and failure. Surface defects (i.e. large voids located on the surface, far exceeding the nominal surface roughness) that were near the primary stress concentration affected the location of crack initiation in some cases, but they did not noticeably affect the global response. The fracture surfaces were a combination of classic ductile dimples and crack deviation from a more direct path favoring intersection with AM voids. Even though the AM voids promoted crack deviation, pre-test micro-CT scan statistics of the voids did not allow for conclusive predictions of preferred crack paths. This study is a first step towards investigating the importance of voids on the ductile failure of AM structures with stress concentrations.

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TYPE Journal Article YEAR 2019
ScopusOSTIDOI

Born Qualified Grand Challenge LDRD Final Report

Roach, R.A.; Argibay, Nicolas A.; Allen, Kyle M.; Balch, Dorian K.; Beghini, Lauren L.; Bishop, Joseph E.; Boyce, Brad B.; Brown, Judith A.; Burchard, Ross L.; Chandross, M.; Cook, Adam W.; DiAntonio, Christopher D.; Dressler, Amber D.; Forrest, Eric C.; Ford, Kurtis R.; Ivanoff, Thomas I.; Jared, Bradley H.; Johnson, Kyle J.; Kammler, Daniel K.; Koepke, Joshua R.; Kustas, Andrew K.; Lavin, Judith M.; Leathe, Nicholas L.; Lester, Brian T.; Madison, Jonathan D.; Mani, Seethambal S.; Martinez, Mario J.; Moser, Daniel M.; Rodgers, Theron R.; Seidl, Daniel T.; Brown-Shaklee, Harlan J.; Stanford, Joshua S.; Stender, Michael S.; Sugar, Joshua D.; Swiler, Laura P.; Taylor, Samantha T.; Trembacki, Bradley T.

This SAND report fulfills the final report requirement for the Born Qualified Grand Challenge LDRD. Born Qualified was funded from FY16-FY18 with a total budget of ~$13M over the 3 years of funding. Overall 70+ staff, Post Docs, and students supported this project over its lifetime. The driver for Born Qualified was using Additive Manufacturing (AM) to change the qualification paradigm for low volume, high value, high consequence, complex parts that are common in high-risk industries such as ND, defense, energy, aerospace, and medical. AM offers the opportunity to transform design, manufacturing, and qualification with its unique capabilities. AM is a disruptive technology, allowing the capability to simultaneously create part and material while tightly controlling and monitoring the manufacturing process at the voxel level, with the inherent flexibility and agility in printing layer-by-layer. AM enables the possibility of measuring critical material and part parameters during manufacturing, thus changing the way we collect data, assess performance, and accept or qualify parts. It provides an opportunity to shift from the current iterative design-build-test qualification paradigm using traditional manufacturing processes to design-by-predictivity where requirements are addressed concurrently and rapidly. The new qualification paradigm driven by AM provides the opportunity to predict performance probabilistically, to optimally control the manufacturing process, and to implement accelerated cycles of learning. Exploiting these capabilities to realize a new uncertainty quantification-driven qualification that is rapid, flexible, and practical is the focus of this effort.

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TYPE SAND Report YEAR 2018
OSTIDOI

Data Analysis for the Born Qualified Grand LDRD Project

Swiler, Laura P.; van Bloemen Waanders, Bart G.; Jared, Bradley H.; Koepke, Joshua R.; Whetten, Shaun R.; Madison, Jonathan D.; Ivanoff, Thomas I.; Jackson, Olivia D.; Cook, Adam W.; Brown-Shaklee, Harlan J.; Kammler, Daniel K.; Johnson, Kyle J.; Ford, Kurtis R.; Bishop, Joseph E.; Roach, R.A.

This report summarizes the data analysis activities that were performed under the Born Qualified Grand Challenge Project from 2016 - 2018. It is meant to document the characterization of additively manufactured parts and processe s for this project as well as demonstrate and identify further analyses and data science that could be done relating material processes to microstructure to properties to performance.

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TYPE SAND Report YEAR 2018
OSTIDOI
39 Results
39 Results