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Thermally-activated pentanol delivery from precursor poly(p- phenylenevinylene)s for MEMS lubrication

Macromolecular Rapid Communications

Johnson, Ross S.; Washburn, Cody M.; Staton, Alan W.; Moorman, Matthew W.; Manginell, Ronald P.; Dugger, Michael T.; Dirk, Shawn M.

The synthesis of two new polyphenylene vinylene (PPV) precursor polymers which can be thermally induced to eliminate pentanol is presented. Pentanol has recently been discovered to be a very useful lubricant in MicroElectroMechanical Systems. The utilization of the elimination reaction of precursor polymers to PPV as a small molecule delivery platform has, to the best of our knowledge, not been previously reported. The elimination reactions were examined using thermal gravimetric analysis, gas chromatography, and UV-Vis spectroscopy. Using PPV precursors allows for (1) a high loading of lubricant (one molecule per monomeric unit), (2) a platform that requires relatively high temperatures (>145 °C) to eliminate the lubricant, and (3) a non-volatile, mechanically and chemically stable by-product of the elimination reaction (PPV). The "on-demand" delivery of a vapor-phase lubricant to MicroElectoMechanical Systems (MEMS) will allow for scheduled or as-needed lubrication of the moving components, improving the performance, reliability, and lifespan of the devices. A delivery system utilizing a newly designed microhotplate along with two new precursor poly(p-phenylene vinylene) polymers that thermally eliminate a pentanol lubricant is described. Copyright © 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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Thermo-switchable polymer dielectrics

Johnson, Ross S.; Dirk, Shawn M.

We are interested in utilizing the thermo-switchable properties of precursor poly(p-phenylene vinylene) (PPV) polymers to develop capacitor dielectrics that will fail at specific temperatures due to the material irreversibly switching from an insulator to a conducting polymer. By utilizing different leaving groups on the polymer main chain, the temperature at which the polymer transforms into a conductor can be varied over a range of temperatures. Electrical characterization of thin-film capacitors prepared from several precursor PPV polymers indicates that these materials have good dielectric properties until they reach elevated temperatures, at which point conjugation of the polymer backbone effectively disables the device. Here, we present the synthesis, dielectric processing, and electrical characterization of a new thermo-switchable polymer dielectric.

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Photo-lithography of xanthate precursor poly(p-phenylenevinylene) polymers

Johnson, Ross S.; Dirk, Shawn M.

Conjugated polymers such as poly(p-phenylenevinylene) (PPV) have attracted a great deal of attention due to their optoelectronic properties. The ability to control the lateral spatial resolution of conjugated polymers will allow for improved integration into electronic devices. Here, we present a method for photo-patterning xanthate precursor polymers leading to micron scale spatial control of conjugated poly(p-phenylenevinylene). Our photolithographic process is simple and direct, and should be amenable to a range of other xanthate or dithiocarbamate precursor PPV polymers.

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Temperature switchable polymer dielectrics

Johnson, Ross S.; Dirk, Shawn M.

Materials with switchable states are desirable in many areas of science and technology. The ability to thermally transform a dielectric material to a conductive state should allow for the creation of electronics with built-in safety features. Specifically, the non-desirable build-up and discharge of electricity in the event of a fire or over-heating would be averted by utilizing thermo-switchable dielectrics in the capacitors of electrical devices (preventing the capacitors from charging at elevated temperatures). We have designed a series of polymers that effectively switch from a non-conductive to a conductive state. The thermal transition is governed by the stability of the leaving group after it leaves as a free entity. Here, we present the synthesis and characterization of a series of precursor polymers that eliminate to form poly(p-phenylene vinylene) (PPV's).

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11 Results
11 Results