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3D optical diagnostics for explosively driven deformation and fragmentation

International Journal of Impact Engineering

Guildenbecher, Daniel R.; Jones, Elizabeth M.; Munz, Elise D.; Reu, Phillip L.; Miller, Timothy J.; Perez, Francisco; Thompson, Andrew D.; Ball, James P.

High-speed, optical imaging diagnostics are presented for three-dimensional (3D) quantification of explosively driven metal fragmentation. At early times after detonation, Digital Image Correlation (DIC) provides non-contact measures of 3D case velocities, strains, and strain rates, while a proposed stereo imaging configuration quantifies in-flight fragment masses and velocities at later times. Experiments are performed using commercially obtained RP-80 detonators from Teledyne RISI, which are shown to create a reproducible fragment field at the benchtop scale. DIC measurements are compared with 3D simulations, which have been ‘leveled’ to match the spatial resolution of DIC. Results demonstrate improved ability to identify predicted quantities-of-interest that fall outside of measurement uncertainty and shot-to-shot variability. Similarly, video measures of fragment trajectories and masses allow rapid experimental repetition and provide correlated fragment size-velocity measurements. Measured and simulated fragment mass distributions are shown to agree within confidence bounds, while some statistically meaningful differences are observed between the measured and predicted conditionally averaged fragment velocities. Together these techniques demonstrate new opportunities to improve future model validation.

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Measuring the Residual Stress and Stress Corrosion Cracking Susceptibility of Additively Manufactured 316L by ASTM G36-94

Corrosion

Karasz, Erin K.; Taylor, Jason M.; Autenrieth, David M.; Reu, Phillip L.; Johnson, Kyle J.; Melia, Michael A.; Noell, Philip N.

Residual stress is a contributor to stress corrosion cracking (SCC) and a common byproduct of additive manufacturing (AM). Here the relationship between residual stress and SCC susceptibility in laser powder bed fusion AM 316L stainless steel was studied through immersion in saturated boiling magnesium chloride per ASTM G36-94. The residual stress was varied by changing the sample height for the as-built condition and additionally by heat treatments at 600°C, 800°C, and 1,200°C to control, and in some cases reduce, residual stress. In general, all samples in the as-built condition showed susceptibility to SCC with the thinner, lower residual stress samples showing shallower cracks and crack propagation occurring perpendicular to melt tracks due to local residual stress fields. The heat-treated samples showed a reduction in residual stress for the 800°C and 1,200°C samples. Both were free of cracks after >300 h of immersion in MgCl2, while the 600°C sample showed similar cracking to their as-built counterpart. Geometrically necessary dislocation (GND) density analysis indicates that the dislocation density may play a major role in the SCC susceptibility.

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Experimental Modal Analysis Using Phase Quantities from Phase-Based Motion Processing and Motion Magnification

Experimental Techniques

Rohe, D.P.; Reu, Phillip L.

Phase-based motion processing and the associated Motion Magnification that it enables has become popular not only for the striking videos that it can produce of traditionally stiff structures visualized with very large deflections, but also for its ability to pull information out of the noise floor of images so that they can be processed with more traditional optical techniques such as digital image correlation or feature tracking. While the majority of papers in the literature have utilized the Phase-based Image Processing approach as a pre-processor for more quantitative analyses, the technique itself can be used directly to extract modal parameters from an image, noting that the extracted phases are proportional to displacements in the image. Once phases are extracted, they can be fit using traditional experimental modal analysis techniques. This produces a mode “shape” where the degrees of freedom are phases instead of physical motions. These phases can be scaled to produce on-image visualizations of the mode shapes, rather than operational shapes produced by bandpass filtering. Modal filtering techniques can also be used to visualize motions from an environment on an image using the modal phases as a basis for the expansion.

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A Generalized Stress Inversion Approach with Application to Residual Stress Estimation

Journal of Applied Mechanics, Transactions ASME

Chen, Mark J.; Aquino, Wilkins A.; Walsh, Timothy W.; Reu, Phillip L.; Johnson, Kyle J.; Rouse, Jerry W.; Jared, Bradley H.; Bishop, Joseph E.

We develop a generalized stress inversion technique (or the generalized inversion method) capable of recovering stresses in linear elastic bodies subjected to arbitrary cuts. Specifically, given a set of displacement measurements found experimentally from digital image correlation (DIC), we formulate a stress estimation inverse problem as a partial differential equation-constrained optimization problem. We use gradient-based optimization methods, and we accordingly derive the necessary gradient and Hessian information in a matrix-free form to allow for parallel, large-scale operations. By using a combination of finite elements, DIC, and a matrix-free optimization framework, the generalized inversion method can be used on any arbitrary geometry, provided that the DIC camera can view a sufficient part of the surface. We present numerical simulations and experiments, and we demonstrate that the generalized inversion method can be applied to estimate residual stress.

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X-Ray Stereo Digital Image Correlation

Experimental Techniques

Jones, Elizabeth M.; Quintana, Enrico C.; Reu, Phillip L.; Wagner, Justin W.

Digital Image Correlation (DIC) is a well-established, non-contact diagnostic technique used to measure shape, displacement and strain of a solid specimen subjected to loading or deformation. However, measurements using standard DIC can have significant errors or be completely infeasible in challenging experiments, such as explosive, combustion, or fluid-structure interaction applications, where beam-steering due to index of refraction variation biases measurements or where the sample is engulfed in flames or soot. To address these challenges, we propose using X-ray imaging instead of visible light imaging for stereo-DIC, since refraction of X-rays is negligible in many situations, and X-rays can penetrate occluding material. Two methods of creating an appropriate pattern for X-ray DIC are presented, both based on adding a dense material in a random speckle pattern on top of a less-dense specimen. A standard dot-calibration target is adapted for X-ray imaging, allowing the common bundle-adjustment calibration process in commercial stereo-DIC software to be used. High-quality X-ray images with sufficient signal-to-noise ratios for DIC are obtained for aluminum specimens with thickness up to 22.2 mm, with a speckle pattern thickness of only 80 μm of tantalum. The accuracy and precision of X-ray DIC measurements are verified through simultaneous optical and X-ray stereo-DIC measurements during rigid in-plane and out-of-plane translations, where errors in the X-ray DIC displacements were approximately 2–10 μm for applied displacements up to 20 mm. Finally, a vast reduction in measurement error—5–20 times reduction of displacement error and 2–3 times reduction of strain error—is demonstrated, by comparing X-ray and optical DIC when a hot plate induced a heterogeneous index of refraction field in the air between the specimen and the imaging systems. Collectively, these results show the feasibility of using X-ray-based stereo-DIC for non-contact measurements in exacting experimental conditions, where optical DIC cannot be used.

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Spatial DIC Errors due to Pattern-Induced Bias and Grey Level Discretization

Experimental Mechanics

Fayad, Samuel S.; Seidl, D.T.; Reu, Phillip L.

Digital image correlation (DIC) is an optical metrology method widely used in experimental mechanics for full-field shape, displacement and strain measurements. The required strain resolution for engineering applications of interest mandates DIC to have a high image displacement matching accuracy, on the order of 1/100th of a pixel, which necessitates an understanding of DIC errors. In this paper, we examine two spatial bias terms that have been almost completely overlooked. They cause a persistent offset in the matching of image intensities and thus corrupt DIC results. We name them pattern-induced bias (PIB), and intensity discretization bias (IDB). We show that the PIB error occurs in the presence of an undermatched shape function and is primarily dictated by the underlying intensity pattern for a fixed displacement field and DIC settings. The IDB error is due to the quantization of the gray level intensity values in the digital camera. In this paper we demonstrate these errors and quantify their magnitudes both experimentally and with synthetic images.

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Development of a Generalized Residual Stress Inversion Technique

Johnson, Kyle J.; Bishop, Joseph E.; Reu, Phillip L.; Walsh, Timothy W.; Farias, Paul A.; Jared, Bradley H.; Susan, D.F.; Rouse, Jerry W.; Whetten, Shaun R.; Chen, Mark J.; Aquino, Wilkins A.; Bellotti, Aurelio B.; Jacobs, Laurence J.

Residual stress is a common result of manufacturing processes, but it is one that is often overlooked in design and qualification activities. There are many reasons for this oversight, such as lack of observable indicators and difficulty in measurement. Traditional relaxation-based measurement methods use some type of material removal to cause surface displacements, which can then be used to solve for the residual stresses relieved by the removal. While widely used, these methods may offer only individual stress components or may be limited by part or cut geometry requirements. Diffraction-based methods, such as X-ray or neutron, offer non-destructive results but require access to a radiation source. With the goal of producing a more flexible solution, this LDRD developed a generalized residual stress inversion technique that can recover residual stresses released by all traction components on a cut surface, with much greater freedom in part geometry and cut location. The developed method has been successfully demonstrated on both synthetic and experimental data. The project also investigated dislocation density quantification using nonlinear ultrasound, residual stress measurement using Electronic Speckle Pattern Interferometry Hole Drilling, and validation of residual stress predictions in Additive Manufacturing process models.

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Investigation of assumptions and approximations in the virtual fields method for a viscoplastic material model

Strain

Jones, Elizabeth M.; Karlson, Kyle N.; Reu, Phillip L.

The Virtual Fields Method (VFM) is an inverse technique used for parameter estimation and calibration of constitutive models. Many assumptions and approximations—such as plane stress, incompressible plasticity, and spatial and temporal derivative calculations—are required to use VFM with full-field deformation data, for example, from Digital Image Correlation (DIC). This work presents a comprehensive discussion of the effects of these assumptions and approximations on parameters identified by VFM for a viscoplastic material model for 304L stainless steel. We generated synthetic data from a Finite-Element Analysis (FEA) in order to have a reference solution with a known material model and known model parameters, and we investigated four cases in which successively more assumptions and approximations were included in the data. We found that VFM is tolerant to small deviations from the plane stress condition in a small region of the sample, and that the incompressible plasticity assumption can be used to estimate thickness changes with little error. A local polynomial fit to the displacement data was successfully employed to compute the spatial displacement gradients. The choice of temporal derivative approximation (i.e., backwards difference versus central difference) was found to have a significant influence on the computed rate of deformation and on the VFM results for the rate-dependent model used in this work. Finally, the noise introduced into the displacement data from a stereo-DIC simulator was found to have negligible influence on the VFM results. Evaluating the effects of assumptions and approximations using synthetic data is a critical first step for verifying and validating VFM for specific applications. The results of this work provide the foundation for confidently using VFM for experimental data.

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Update on the 2D-DIC challenge: Results and conclusions

Conference Proceedings of the Society for Experimental Mechanics Series

Reu, Phillip L.; Toussaint, E.; Jones, E.; Bruck, H.; Iadicola, M.; Balcaen, R.; Turner, Daniel Z.; Siebert, T.; Lava, P.; Simonsen, M.; Grewer, M.

The 2D-DIC Challenge is organized by an international committee working to understand the accuracy of digital image correlation (DIC) through standardized image sets. The DIC Challenge is run under the auspices of the Society for Experimental Mechanics (SEM) and the International DIC Society (iDICs). The 2D-Challenge incorporates 19 image sets that can be used in evaluating 2D-DIC algorithms. The full results of the study and description of the image sets may be found in Reu et al. (Exp Mech, 2017). A new round of the 2D Challenge is being launched at SEM 2018 and will seek to probe the concept of spatial resolution.

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Eliminating air refraction issues in DIC by conducting experiments in vacuum

Conference Proceedings of the Society for Experimental Mechanics Series

Reu, Phillip L.; Jones, Elizabeth M.

A major and often unrecognized error source in digital image correlation (DIC) is the influence of the intervening air between the cameras and sample. Minute differences in air temperature, composition, or both can cause index of refraction changes that act as a lens and cause distortions in the DIC displacement and strain results (Jones and Reu, Exp Mech, 2017). There are limited options to correct this problem as it is both spatial and temporal in nature. One method is to use X-rays for imaging that are not affected by air refraction, but this requires costly equipment. A second method uses a vacuum chamber to minimize the intervening air to remove the distortions, but unfortunately this requires inconvenient setups.

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Distortion of Digital Image Correlation (DIC) Displacements and Strains from Heat Waves

Experimental Mechanics

Jones, Elizabeth M.; Reu, Phillip L.

“Heat waves” is a colloquial term used to describe convective currents in air formed when different objects in an area are at different temperatures. In the context of Digital Image Correlation (DIC) and other optical-based image processing techniques, imaging an object of interest through heat waves can significantly distort the apparent location and shape of the object. There are many potential heat sources in DIC experiments, including but not limited to lights, cameras, hot ovens, and sunlight, yet error caused by heat waves is often overlooked. This paper first briefly presents three practical situations in which heat waves contributed significant error to DIC measurements to motivate the investigation of heat waves in more detail. Then the theoretical background of how light is refracted through heat waves is presented, and the effects of heat waves on displacements and strains computed from DIC are characterized in detail. Finally, different filtering methods are investigated to reduce the displacement and strain errors caused by imaging through heat waves. The overarching conclusions from this work are that errors caused by heat waves are significantly higher than typical noise floors for DIC measurements, and that the errors are difficult to filter because the temporal and spatial frequencies of the errors are in the same range as those of typical signals of interest. Therefore, eliminating or mitigating the effects of heat sources in a DIC experiment is the best solution to minimizing errors caused by heat waves.

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Parameter covariance and non-uniqueness in material model calibration using the Virtual Fields Method

Computational Materials Science

Jones, Elizabeth M.; Carroll, Jay D.; Karlson, Kyle N.; Kramer, S.L.B.; Lehoucq, Richard B.; Reu, Phillip L.; Turner, Daniel Z.

Traditionally, material identification is performed using global load and displacement data from simple boundary-value problems such as uni-axial tensile and simple shear tests. More recently, however, inverse techniques such as the Virtual Fields Method (VFM) that capitalize on heterogeneous, full-field deformation data have gained popularity. In this work, we have written a VFM code in a finite-deformation framework for calibration of a viscoplastic (i.e. strain-rate dependent) material model for 304L stainless steel. Using simulated experimental data generated via finite-element analysis (FEA), we verified our VFM code and compared the identified parameters with the reference parameters input into the FEA. The identified material model parameters had surprisingly large error compared to the reference parameters, which was traced to parameter covariance and the existence of many essentially equivalent parameter sets. This parameter non-uniqueness and its implications for FEA predictions is discussed in detail. Finally, we present two strategies to reduce parameter covariance – reduced parametrization of the material model and increased richness of the calibration data – which allow for the recovery of a unique solution.

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DIC Challenge: Developing Images and Guidelines for Evaluating Accuracy and Resolution of 2D Analyses

Experimental Mechanics

Reu, Phillip L.; Toussaint, E.; Jones, E.; Bruck, H.A.; Iadicola, M.; Balcaen, R.; Turner, Daniel Z.; Siebert, T.; Lava, P.; Simonsen, M.

With the rapid spread in use of Digital Image Correlation (DIC) globally, it is important there be some standard methods of verifying and validating DIC codes. To this end, the DIC Challenge board was formed and is maintained under the auspices of the Society for Experimental Mechanics (SEM) and the international DIC society (iDICs). The goal of the DIC Board and the 2D–DIC Challenge is to supply a set of well-vetted sample images and a set of analysis guidelines for standardized reporting of 2D–DIC results from these sample images, as well as for comparing the inherent accuracy of different approaches and for providing users with a means of assessing their proper implementation. This document will outline the goals of the challenge, describe the image sets that are available, and give a comparison between 12 commercial and academic 2D–DIC codes using two of the challenge image sets.

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High-throughput Material Characterization using the Virtual Fields Method

Jones, Elizabeth M.; Carroll, Jay D.; Karlson, Kyle N.; Kramer, Sharlotte L.; Lehoucq, Richard B.; Reu, Phillip L.; Seidl, Daniel T.; Turner, Daniel Z.

Modeling material and component behavior using finite element analysis (FEA) is critical for modern engineering. One key to a credible model is having an accurate material model, with calibrated model parameters, which describes the constitutive relationship between the deformation and the resulting stress in the material. As such, identifying material model parameters is critical to accurate and predictive FEA. Traditional calibration approaches use only global data (e.g. extensometers and resultant force) and simplified geometries to find the parameters. However, the utilization of rapidly maturing full-field characterization tech- niques (e.g. Digital Image Correlation (DIC)) with inverse techniques (e.g. the Virtual Feilds Method (VFM)) provide a new, novel and improved method for parameter identification. This LDRD tested that idea: in particular, whether more parameters could be identified per test when using full-field data. The research described in this report successfully proves this hypothesis by comparing the VFM results with traditional calibration methods. Important products of the research include: verified VFM codes for identifying model parameters, a new look at parameter covariance in material model parameter estimation, new validation tech- niques to better utilize full-field measurements, and an exploration of optimized specimen design for improved data richness.

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The Effect of the Ill-posed Problem on Quantitative Error Assessment in Digital Image Correlation

Experimental Mechanics

Turner, Daniel Z.; Lehoucq, Richard B.; Reu, Phillip L.

Here, this work explores the effect of the ill-posed problem on uncertainty quantification for motion estimation using digital image correlation (DIC) (Sutton et al. 2009). We develop a correction factor for standard uncertainty estimates based on the cosine of the angle between the true motion and the image gradients, in an integral sense over a subregion of the image. This correction factor accounts for variability in the DIC solution previously unaccounted for when considering only image noise, interpolation bias, contrast, and the software settings such as subset size and spacing.

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A speckle patterning study for laboratory-scale DIC experiments

Conference Proceedings of the Society for Experimental Mechanics Series

Kramer, Sharlotte L.; Reu, Phillip L.; Bonk, Sarah

A “good” speckle pattern enables DIC to make its full-field measurements, but oftentimes this artistic part of the DIC setup takes a considerable amount of time to develop and evaluate for a given optical configuration. A catalog of well-quantified speckle patterns for various fields of view would greatly decrease the time it would take to start making DIC measurements. The purpose of this speckle patterning study is to evaluate various speckling techniques we had readily available in our laboratories for fields of view from around 100 mm down to 5 mm that are common for laboratory-scale experiments. The list of speckling techniques is not exhaustive: spray painting, UV-printing of computer-designed speckle patterns, airbrushing, and particle dispersion. First, we quantified the resolution of our optical configurations for each of the fields of view to determine the smallest speckle we could resolve. Second, we imaged several speckle patterns at each field of view. Third, we quantified the average and standard deviation of the speckle size, speckle contrast, and density to characterize the quality of the speckle pattern. Finally, we performed computer-aided sub-pixel translation of the speckle patterns and ran correlations to examine how well DIC tracked the pattern translations. We discuss our metrics for a “good” speckle pattern and outline how others may perform similar studies for their desired optical configurations.

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A nonlocal strain measure for DIC

Conference Proceedings of the Society for Experimental Mechanics Series

Turner, Daniel Z.; Lehoucq, Richard B.; Reu, Phillip L.

It is well known that the derivative-based classical approach to strain is problematic when the displacement field is irregular, noisy, or discontinuous. Difficulties arise wherever the displacements are not differentiable. We present an alternative, nonlocal approach to calculating strain from digital image correlation (DIC) data that is well-defined and robust, even for the pathological cases that undermine the classical strain measure. This integral formulation for strain has no spatial derivatives and when the displacement field is smooth, the nonlocal strain and the classical strain are identical. We submit that this approach to computing strains from displacements will greatly improve the fidelity and efficacy of DIC for new application spaces previously untenable in the classical framework.

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A realistic error budget for two dimension digital image correlation

Conference Proceedings of the Society for Experimental Mechanics Series

Reu, Phillip L.

There has been a lot of interest in the matching error for two-dimensional digital image correlation (2D-DIC), including the matching bias and variance; however, there are a number of other sources of error that must also be considered. These include temperature drift of the camera, out-of-plane sample motion, lack of perpendicularity, under-matched subset shape functions, and filtering of the results during the strain calculation. This talk will use experimental evidence to demonstrate some of the ignored error sources and compile a complete “notional” error budget for a typical 2D measurement.

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High-speed stereomicroscope digital image correlation of rupture disc behavior

Conference Proceedings of the Society for Experimental Mechanics Series

Cooper, Marcia A.; Skaggs, Michelle N.; Reu, Phillip L.

Three-dimensional deformation of rupture discs subjected to gas-dynamic shock loading was measured using a stereomicroscope digital image correlation (DIC) system. One-dimensional blast waves generated with a small-diameter, explosively driven shock tube were used for studying the fluid-structure interactions that exist when incident onto relatively low-strength rupture discs. Prior experiments have shown that subjecting the 0. 64-cm-diameter, stainless steel rupture discs to shock waves of varying strength results in a range of responses from no rupture to shear at the outer weld diameter. In this work, the outer surface of the rupture discs were prepared for DIC using 100–150 _m-sized speckles and illuminated with a Xenon flashlamp. Two synchronized Shimadzu HPV-2 cameras coupled to an Olympus microscope captured stereoimage sequences of rupture disc behavior at speeds of 1 MHz. Image correlation performed on the stereo-images resulted in spatially resolved surface deformation. The experimental facility, specifics of the DIC diagnostic technique, and the temporal deformation and velocity of the surface of a rupturing disc are presented.

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Virtual strain gage size study

Experimental Techniques

Reu, Phillip L.

DIC is a non-linear low-pass spatial filtering operation; whether we consider the effect of the subset and shape function, the strain window used in the strain calculation, of other post-processing of the results, each decision will impact the spatial resolution, of the measurement. More fundamentally, the speckle size limits, the spatial resolution by dictating the smallest possible subset. After this decision the processing settings are controlled by the allowable noise level balanced by possible bias errors created by the data filtering. This article describes a process to determine optimum DIC software settings to determine if the peak displacements or strains are being found.

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Ductile Tearing of Thin Aluminum Plates Under Blast Loading. Predictions with Fully Coupled Models and Biaxial Material Response Characterization

Corona, Edmundo C.; Gullerud, Arne S.; Haulenbeek, Kimberly K.; Reu, Phillip L.

The work presented in this report concerns the response and failure of thin 2024- T3 aluminum alloy circular plates to a blast load produced by the detonation of a nearby spherical charge. The plates were fully clamped around the circumference and the explosive charge was located centrally with respect to the plate. The principal objective was to conduct a numerical model validation study by comparing the results of predictions to experimental measurements of plate deformation and failure for charges with masses in the vicinity of the threshold between no tearing and tearing of the plates. Stereo digital image correlation data was acquired for all tests to measure the deflection and strains in the plates. The size of the virtual strain gage in the measurements, however, was relatively large, so the strain measurements have to be interpreted accordingly as lower bounds of the actual strains in the plate and of the severity of the strain gradients. A fully coupled interaction model between the blast and the deflection of the structure was considered. The results of the validation exercise indicated that the model predicted the deflection of the plates reasonably accurately as well as the distribution of strain on the plate. The estimation of the threshold charge based on a critical value of equivalent plastic strain measured in a bulge test, however, was not accurate. This in spite of efforts to determine the failure strain of the aluminum sheet under biaxial stress conditions. Further work is needed to be able to predict plate tearing with some degree of confidence. Given the current technology, at least one test under the actual blast conditions where the plate tears is needed to calibrate the value of equivalent plastic strain when failure occurs in the numerical model. Once that has been determined, the question of the explosive mass value at the threshold could be addressed with more confidence.

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Evaluation of various interpolants available in DICE

Turner, Daniel Z.; Reu, Phillip L.; Crozier, Paul C.

This report evaluates several interpolants implemented in the Digital Image Correlation Engine (DICe), an image correlation software package developed by Sandia. By interpolants we refer to the basis functions used to represent discrete pixel intensity data as a continuous signal. Interpolation is used to determine intensity values in an image at non - pixel locations. It is also used, in some cases, to evaluate the x and y gradients of the image intensities. Intensity gradients subsequently guide the optimization process. The goal of this report is to inform analysts as to the characteristics of each interpolant and provide guidance towards the best interpolant for a given dataset. This work also serves as an initial verification of each of the interpolants implemented.

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Camera System Resolution and its Influence on Digital Image Correlation

Experimental Mechanics

Reu, Phillip L.; Sweatt, W.C.; Miller, T.; Fleming, Darryn F.

Digital image correlation (DIC) uses images from a camera and lens system to make quantitative measurements of the shape, displacement, and strain of test objects. This increasingly popular method has had little research on the influence of the imaging system resolution on the DIC results. This paper investigates the entire imaging system and studies how both the camera and lens resolution influence the DIC results as a function of the system Modulation Transfer Function (MTF). It will show that when making spatial resolution decisions (including speckle size) the resolution limiting component should be considered. A consequence of the loss of spatial resolution is that the DIC uncertainties will be increased. This is demonstrated using both synthetic and experimental images with varying resolution. The loss of image resolution and DIC accuracy can be compensated for by increasing the subset size, or better, by increasing the speckle size. The speckle-size and spatial resolution are now a function of the lens resolution rather than the more typical assumption of the pixel size. The paper will demonstrate the tradeoffs associated with limited lens resolution.

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Using sampling moiré to extract displacement information from X-Ray images of molten salt batteries

Conference Proceedings of the Society for Experimental Mechanics Series

Reu, Phillip L.; Quintana, Enrico C.; Long, Kevin N.

Full-field axial deformation within molten-salt batteries was measured using x-ray imaging with a sampling moiré technique. This method worked for in situ testing of the batteries because of the inherent grid pattern of the battery layers when imaged with x-rays. High-speed x-ray imaging acquired movies of the layer deformation during battery activation. Numerical validation of the technique, as implemented in this paper, was done using synthetic and numerically shifted images. Typical results of a battery are shown for one test. Ongoing work on validation and more test results are in progress.

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Digital in-line holography to quantify secondary droplets from the impact of a single drop on a thin film

Experiments in Fluids

Guildenbecher, Daniel R.; Engvall, Luke; Gao, Jian; Grasser, Thomas W.; Reu, Phillip L.; Chen, Jun

Digital in-line holography (DIH) is an optical technique which measures particle sizes and their three-dimensional (3D) positions and velocities. Here DIH and a recently proposed hybrid method of particle detection are applied to quantify the secondary droplets generated by the impact of a single drop on a thin film. By leveraging the expected symmetry between in-plane and out-of-plane velocities, experimental depth uncertainty is measured to be approximately 0.7 of the mean droplet diameter. Furthermore, comparison with previous measurements using alternative techniques shows good agreement with the measured temporal evolution of drop number, size, and velocity components. Finally, the power of DIH to extract the complex 3D morphology of the protruding jets is demonstrated. © 2014 Springer-Verlag Berlin Heidelberg.

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A method for overlapping two DIC views by using a two-tone speckle pattern

Conference Proceedings of the Society for Experimental Mechanics Series

Reu, Phillip L.

Because both the accuracy and spatial resolution of digital image correlation (DIC) are directly related to the field-of-view and the number of pixels, it is sometimes advantageous to have a tight view for high resolution measurements and a wide view for overall object deformation. This approach will be demonstrated using a high-speed measurement of the deformation and strain of a riveted thin plate with an explosive loading. Overall plate deformation was provided by a wide-view stereo system, while a tight view of a section of the rivets was imaged with a second stereo pair to measure the strain around the rivet holes. The challenge is creating a speckle pattern which will work with both systems without creating holes in the overall measurement data. This was accomplished by creating a black/white course pattern for the wide view and a black/grey/white fine pattern for the tight view. The grey speckles were sized such that they are not resolved by the wide view and therefore do not compromise the full-field measurement. Details of the process and example results will be presented. © The Society for Experimental Mechanics, Inc. 2014.

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C6 plate puncture testing report

VanGoethem, Doug; Córdova, Theresa E.; Reu, Phillip L.

There are numerous scenarios where critical systems could be subject to penetration by projectiles or fixed objects (e.g., collision, natural disaster, act of terrorism, etc.). It is desired to use computational models to examine these scenarios and make risk-informed decisions; however, modeling of material failure is an active area of research, and new models must be validated with experimental data. The purpose of this report is to document the experimental work performed from FY07 through FY08 on the Campaign Six Plate Puncture project. The goal of this project was to acquire experimental data on the puncture and penetration of metal plates for use in model validation. Of particular interest is the PLH failure model also known as the multilinear line segment model. A significant amount of data that will be useful for the verification and validation of computational models of ductile failure were collected during this project were collected and documented herein; however, much more work remains to be performed, collecting additional experimental data that will further the task of model verification.

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Digital holography simulations and experiments to quantify the accuracy of 3D particle location and 2D sizing using a proposed hybrid method

Applied Optics

Guildenbecher, Daniel R.; Reu, Phillip L.

The accuracy of digital in-line holography to detect particle position and size within a 3D domain is evaluated with particular focus placed on detection of nonspherical particles. Dimensionless models are proposed for simulation of holograms from single particles, and these models are used to evaluate the uncertainty of existing particle detection methods. From the lessons learned, a new hybrid method is proposed. This method features automatic determination of optimum thresholds, and simulations indicate improved accuracy compared to alternative methods. To validate this, experiments are performed using quasi-stationary, 3D particle fields with imposed translations. For the spherical particles considered in experiments, the proposed hybrid method resolves mean particle concentration and size to within 4% of the actual value, while the standard deviation of particle depth is less than two particle diameters. Initial experimental results for nonspherical particles reveal similar performance.

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Damage predictions of aluminum thin-walled structures subjected to explosive loads

Gruda, Jeffrey D.; Corona, Edmundo C.; Gwinn, Kenneth W.; Phelan, James M.; Saul, WVenner S.; Reu, Phillip L.; Stofleth, Jerome H.; Haulenbeek, Kimberly K.; Larsen, Marvin E.

Predicting failure of thin-walled structures from explosive loading is a very complex task. The problem can be divided into two parts; the detonation of the explosive to produce the loading on the structure, and secondly the structural response. First, the factors that affect the explosive loading include: size, shape, stand-off, confinement, and chemistry of the explosive. The goal of the first part of the analysis is predicting the pressure on the structure based on these factors. The hydrodynamic code CTH is used to conduct these calculations. Secondly, the response of a structure from the explosive loading is predicted using a detailed finite element model within the explicit analysis code Presto. Material response, to failure, must be established in the analysis to model the failure of this class of structures; validation of this behavior is also required to allow these analyses to be predictive for their intended use. The presentation will detail the validation tests used to support this program. Validation tests using explosively loaded aluminum thin flat plates were used to study all the aspects mentioned above. Experimental measurements of the pressures generated by the explosive and the resulting plate deformations provided data for comparison against analytical predictions. These included pressure-time histories and digital image correlation of the full field plate deflections. The issues studied in the structural analysis were mesh sensitivity, strain based failure metrics, and the coupling methodologies between the blast and structural models. These models have been successfully validated using these tests, thereby increasing confidence of the results obtained in the prediction of failure thresholds of complex structures, including aircraft.

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Digital image correlation through a rigid borescope

Reu, Phillip L.

There occasionally occur situations in field measurements where direct optical access to the area of interest is not possible. In these cases the borescope is the standard method of imaging. Furthermore, if shape, displacement, or strain are desired in these hidden locations, it would be advantageous to be able to do digital image correlation (DIC) through the borescope. This paper will present the added complexities and errors associated with imaging through a borescope for DIC. Discussion of non-radial distortions and their effects on the measurements, along with a possible correction scheme will be discussed.

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Ultra-high speed imaging and DIC for explosive system observation

Reu, Phillip L.; Cooper, Marcia A.

Digital image correlation (DIC) and the tremendous advances in optical imaging are beginning to revolutionize explosive and high-strain rate measurements. This paper presents results obtained from metallic hemispheres expanded at detonation velocities. Important aspects of sample preparation and lighting of the image will be presented that are key considerations in obtaining images for DIC with frame rates at 1-million frames/second. Quantitative measurements of the case strain rate, expansion velocity and deformation will be presented. Furthermore, preliminary estimations of the measurement uncertainty will be discussed with notes on how image noise and contrast effect the measurement of shape and displacement. The data are then compared with analytical representations of the experiment.

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Experimental validation of 2D uncertainty quantification for DIC

Reu, Phillip L.

Because digital image correlation (DIC) has become such an important and standard tool in the toolbox of experimental mechanicists, a complete uncertainty quantification of the method is needed. It should be remembered that each DIC setup and series of images will have a unique uncertainty based on the calibration quality and the image and speckle quality of the analyzed images. Any pretest work done with a calibrated DIC stereo-rig to quantify the errors using known shapes and translations, while useful, do not necessarily reveal the uncertainty of a later test. This is particularly true with high-speed applications where actual test images are often less than ideal. Work has previously been completed on the mathematical underpinnings of DIC uncertainty quantification and is already published, this paper will present corresponding experimental work used to check the validity of the uncertainty equations.

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Experimental validation of equations for 2D DIC uncertainty quantification

Reu, Phillip L.

Uncertainty quantification (UQ) equations have been derived for predicting matching uncertainty in two-dimensional image correlation a priori. These equations include terms that represent the image noise and image contrast. Researchers at the University of South Carolina have extended previous 1D work to calculate matching errors in 2D. These 2D equations have been coded into a Sandia National Laboratories UQ software package to predict the uncertainty for DIC images. This paper presents those equations and the resulting error surfaces for trial speckle images. Comparison of the UQ results with experimentally subpixel-shifted images is also discussed.

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Experimental validation of 2D uncertainty quantification for digital image correlation

Reu, Phillip L.

Because digital image correlation (DIC) has become such an important and standard tool in the toolbox of experimental mechanicists, a complete uncertainty quantification of the method is needed. It should be remembered that each DIC setup and series of images will have a unique uncertainty based on the calibration quality and the image and speckle quality of the analyzed images. Any pretest work done with a calibrated DIC stereo-rig to quantify the errors using known shapes and translations, while useful, do not necessarily reveal the uncertainty of a later test. This is particularly true with high-speed applications where actual test images are often less than ideal. Work has previously been completed on the mathematical underpinnings of DIC uncertainty quantification and is already published, this paper will present corresponding experimental work used to check the validity of the uncertainty equations.

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Measurement of steel plate perforation tests with digital image correlation

Society for Experimental Mechanics - SEM Annual Conference and Exposition on Experimental and Applied Mechanics 2009

Reu, Phillip L.; VanGoethem, Doug; Córdova, Theresa E.

The results of a series of punch-through tests performed on steel plates are presented. The geometry consisted of circular plates with welded boundary condition penetrated by a conical shaped punch with either a spherical or flat cylindrical end. After initial failure, the conical portion of the punch was driven through the plate to exercise tearing mechanics. Tests were performed quasi-statically with a hydraulic actuator and dynamically using a high-capacity drop table. Deformation and strain were measured with a stereo DIC system. The quasi-static tests utilized a conventional direct-view DIC technique while the dynamic tests required development of an indirect-view technique using a mirror. Experimental details used to conduct the test series will be presented along with test results. Methods of assessing test-to-test repeatability will be discussed. DIC results will also be synchronized and compared with transducer data (displacement and strain). ©2009 Society for Experimental Mechanics Inc.

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Doppler electron velocimeter-practical considerations for a useful tool

Society for Experimental Mechanics - 11th International Congress and Exhibition on Experimental and Applied Mechanics 2008

Reu, Phillip L.

The Doppler electron velocimeter (DEV) is a potentially new dynamic measurement system for the nano-scale. Electron microscopes have been used for many years now for visualizing extremely small samples, but the ability to make dynamic measurements has not existed. The DEV proceeds along the analogous lines of a laser Doppler velocimeter, which uses the Doppler shift of the wave to detect the velocity. The use of electron beams with their extremely short wavelengths overcomes the diffraction limit of light of approximately 1/2-micron to measure samples of current scientific interest in the nano-regime. Previous work has shown that Doppler shifting of electrons is theoretically possible, this paper examines whether a practical instrument can be built given inherent limitations of using electron beams as a probe source. Potential issues and their solutions, including electron beam coherence and interference will be presented. If answers to these problems can be found, the invention of the Doppler electron velocimeter could yield a completely new measurement concept at atomistic scales. © 2008 Society for Experimental Mechanics Inc.

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Doppler electron velocimetry : notes on creating a practical tool

Reu, Phillip L.

The Doppler electron velocimeter (DEV) has been shown to be theoretically possible. This report attempts to answer the next logical question: Is it a practical instrument? The answer hinges upon whether enough electrons are available to create a time-varying Doppler current to be measured by a detector with enough sensitivity and bandwidth. The answer to both of these questions is a qualified yes. A target Doppler frequency of 1 MHz was set as a minimum rate of interest. At this target a theoretical beam current signal-to-noise ratio of 25-to-1 is shown for existing electron holography equipment. A detector is also demonstrated with a bandwidth of 1-MHz at a current of 10 pA. Additionally, a Linnik-type interferometer that would increase the available beam current is shown that would offer a more flexible arrangement for Doppler electron measurements over the traditional biprism.

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Doppler electron velocimeter - A proposed nano-scale dynamic measurement system

Proceedings of the SEM Annual Conference and Exposition on Experimental and Applied Mechanics 2007

Reu, Phillip L.

As engineering challenges grow in the ever shrinking world of nano-design, methods of making dynamic measurements of these materials and systems will become important. Electron microscopes have imaged these extremely small samples for years, but are incapable of measuring dynamic events. A means of measuring these nano-scale dynamic events is envisioned by converting an electron microscope into a Doppler velocimeter. This idea proceeds from the analogous concept of laser Doppler velocimetry. However, the obvious solution of using a laser to probe at the nano-scale is not feasible because the diffraction limit of light is orders of magnitude larger than the samples of interest. This paper investigates the theoretical underpinnings of using electron beams for Doppler measurements. Potential issues and their solutions, including electron beam coherence and interference will be presented. If answers to these problems can be found, the invention of the Doppler electron velocimeter could yield a completely new measurement concept at atomistic scales.

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The Proposed Doppler Electron Velocimeter and the Need for Nanoscale Dynamics

Microscopy Today

Reu, Phillip L.

As engineering challenges grow in the ever-shrinking world of nano-design, methods of making dynamic measurements of nano-materials and systems become more important. The Doppler electron velocimeter (DEV) is a new measurement concept motivated by the increasing importance of nano-dynamics. Nano-dynamics is defined in this context as any phenomenon that causes a dynamically changing phase in an electron beam, and includes traditional mechanical motion, as well as additional phenomena including changing magnetic and electric fields. The DEV is only a theoretical device at this point. Lastly, this article highlights the importance of pursuing nano-dynamics and presents a case that the electron microscope and its associated optics are a viable test bed to develop this new measurement tool.

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Development of the doppler electron velocimeter: theory

Reu, Phillip L.

Measurement of dynamic events at the nano-scale is currently impossible. This paper presents the theoretical underpinnings of a method for making these measurements using electron microscopes. Building on the work of Moellenstedt and Lichte who demonstrated Doppler shifting of an electron beam with a moving electron mirror, further work is proposed to perfect and utilize this concept in dynamic measurements. Specifically, using the concept of ''fringe-counting'' with the current principles of transmission electron holography, an extension of these methods to dynamic measurements is proposed. A presentation of the theory of Doppler electron wave shifting is given, starting from the development of the de Broglie wave, up through the equations describing interference effects and Doppler shifting in electron waves. A mathematical demonstration that Doppler shifting is identical to the conceptually easier to understand idea of counting moving fringes is given by analogy to optical interferometry. Finally, potential developmental experiments and uses of a Doppler electron microscope are discussed.

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Analytical and experimental studies of orthotropic corner-supported plates with segmented in-plane actuators

American Society of Mechanical Engineers, Dynamic Systems and Control Division (Publication) DSC

Sumali, Hartono S.; Massad, Jordan M.; Reu, Phillip L.; Chaplya, Pavel; Martin, Jeffrey W.

This paper outlines a model for a corner-supported, thin, rectangular bimorph actuated by a two-dimensional array of segmented, orthotropic PVDF laminates; it investigates the realization and measurement of such a bimorph. First, a model is derived to determine the deflected shape of an orthotropic laminate for a given distribution of voltages over the actuator array. Then, boundary conditions are realized in a laboratory setup to approach the theoretical corner-supported boundary condition. Finally, deflection measurements of actuated orthotropic PVDF laminates are performed with Electronic Speckle Pattern Interferometry and are compared to the model results. Copyright © 2005 by ASME.

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