Publications

Abstract not provided.

Abstract not provided.

Knowing when, why, and how materials evolve, degrade, or fail in radiation environments is pivotal to a wide range of fields from semiconductor processing to advanced nuclear reactor design. A variety of methods, including optical and electron microscopy, mechanical testing, and thermal techniques, have been used in the past to successfully monitor the microstructural and property evolution of materials exposed to extreme radiation environments.Acoustic techniques have also been used in the past for this purpose, although most methodologies have not achieved widespread adoption. However, with an increasing desire to understand microstructure and property evolution in situ, acoustic methods provide a promising pathway to uncover information not accessible to more traditional characterization techniques. This work highlights how two different classes of acoustic techniques may be used to monitor material evolution during in situ ion beam irradiation. The passive listening technique of acoustic emission is demonstrated on two model systems, quartz and palladium, and shown to be a useful tool in identifying the onset of damage events such as microcracking.An active acoustic technique in the form of transient grating spectroscopy is used to indirectly monitor the formation of small defect clusters in copper irradiated with self-ions at high temperature through the evolution of surface acoustic wave speeds.These studies together demonstrate the large potential for using acoustic techniques as in situ diagnostics. Such tools could be used to optimize ion beam processing techniques or identify modes and kinetics of materials degradation in extreme radiation environments.

Abstract not provided.

Abstract not provided.

Measuring the size and orientation of borehole breakouts is one of the primary methods for determining the orientation and magnitudes of the in situ stresses in the subsurface. To better understand the effects of anisotropy on borehole breakouts, experiments were conducted on Mancos Shale, a finely laminated mudrock. A novel testing configuration was developed to conduct borehole breakout experiments in a standard triaxial vessel and load frame. Samples were prepared at three different orientations and deformed under 6.9 to 20.7 MPa confining pressure. The results show a variation of peak strength and breakout geometry depending on the lamination orientation. Samples deformed parallel to laminations failed at a higher maximum compressive stress than samples deformed perpendicular to laminations, which were stronger than inclined samples. These relationships are quantified by a cosine-based failure envelope. Observed breakout shapes in perpendicular samples are V-shaped and symmetric around the borehole, which advance as a series of fractures of increasing size into the sidewalls. In inclined samples, fractures form along weaker laminations planes and grow in an en echelon pattern towards the axial stress direction. In parallel samples, long fractures grow from the wellbore towards the axial stress direction. The observed geometries highlight potential sources of error in calculating in situ stresses from borehole breakouts.

Abstract not provided.

Abstract not provided.

Abstract not provided.

The purpose of this ISRM Suggested Method is to introduce a guideline on determining deformation and failure characteristics of rocks subjected to true triaxial compression on different stress path. The true triaxial testing apparatus was reviewed by means of the function and engineering application. Some key techniques, such as stress and strain measurements, and reduction of end effect between specimen and metal platens, preventing metal platens interference, were stated and suggested in detail. Methodology of specimen processing, specimen shape, and testing procedure are characterized. There is an explanation of the experimental data processing on stress–strain curves, strength, and fracture mode.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

A novel experimental geometry is combined with acoustic emission monitoring capability to measure crack growth and damage accumulation during laboratory simulations of borehole breakout. Three different experiments are conducted in this study using Sierra White Granite. In the first experiment, the sample is deformed at a constant 17.2 MPa confining pressure without pore fluids; in the second experiment, the sample is held at a constant effective pressure of 17.2 MPa with a constant pore pressure; and in the third experiment, pore pressure is modified to induce failure at otherwise constant stress. The results demonstrate that effective pressure and stress path have controlling influence on breakout initiation and damage accumulation in laboratory simulations of wellbore behavior. Excellent agreement between the dry test and constant pore pressure test verify the application of the effective pressure law to borehole deformation. Located AE events coincide with post-test observations of damage and fracture locations. Comparison of AE behavior between the experiments with pore pressure show that breakouts develop prior to peak stress, and continued loading drives damage further into the formation and generates shear fractures.

We generate a wide range of models of proppant-packed fractures using discrete element simulations, and measure fracture conductivity using finite element flow simulations. This allows for a controlled computational study of proppant structure and its relationship to fracture conductivity and stress in the proppant pack. For homogeneous multi-layered packings, we observe the expected increase in fracture conductivity with increasing fracture aperture, while the stress on the proppant pack remains nearly constant. This is consistent with the expected behavior in conventional proppant-packed fractures, but the present work offers a novel quantitative analysis with an explicit geometric representation of the proppant particles. In single-layered packings (i.e. proppant monolayers), there is a drastic increase in fracture conductivity as the proppant volume fraction decreases and open flow channels form. However, this also corresponds to a sharp increase in the mechanical stress on the proppant pack, as measured by the maximum normal stress relative to the side crushing strength of typical proppant particles. We also generate a variety of computational geometries that resemble highly heterogeneous proppant packings hypothesized to form during channel fracturing. In some cases, these heterogeneous packings show drastic improvements in conductivity with only moderate increase in the stress on the proppant particles, suggesting that in certain applications these structures are indeed optimal. We also compare our computer-generated structures to micro computed tomography imaging of a manually fractured laboratory-scale shale specimen, and find reasonable agreement in the geometric characteristics.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Results of axisymmetric compression tests on weak, porous Castlegate Sandstone (Cretaceous, Utah, USA), covering a range of dilational and compactional behaviors, are examined for localization behavior. Assuming isotropy, bulk and shear moduli evolve as increasing functions of mean stress and Mises equivalent shear stress respectively, and as decreasing functions of work-conjugate plastic strains. Acoustic emissions events located during testing show onset of localization and permit calculation of observed shear and low-angle compaction localization zones, or bands, as localization commences. Total strain measured experimentally partitions into: A) elastic strain with constant moduli, B) elastic strain due to stress dependence of moduli, C) elastic strain due to moduli degradation with increasing plastic strain, and D) plastic strain. The third term is the elastic-plastic coupling strain, and though often ignored, contributes significantly to pre-failure total strain for brittle and transitional tests. Constitutive parameters and localization predictions derived from experiments are compared to theoretical predictions. In the brittle regime, predictions of band angles (angle between band normal and maximum compression) demonstrate good agreement with observed shear band angles. Compaction localization was observed in the transitional regime in between shear localization and spatially pervasive compaction, over a small range of mean stresses. In contrast with predictions, detailed acoustic emissions analyses in this regime show low angle, compaction-dominated but shear-enhanced, localization.

For assessing energy-related activities in the subsurface, it is important to investigate the impact of the spatial variability and anisotropy on the geomechanical behavior of shale. The Brazilian test, an indirect tensile-splitting method, is performed in this work, and the evolution of strain field is obtained using digital image correlation. Experimental results show the significant impact of local heterogeneity and lamination on the crack pattern characteristics. For numerical simulations, a phase field method is used to simulate the brittle fracture behavior under various Brazilian test conditions. In this study, shale is assumed to consist of two constituents including the stiff and soft layers to which the same toughness but different elastic moduli are assigned. Microstructural heterogeneity is simplified to represent mesoscale (e.g., millimeter scale) features such as layer orientation, thickness, volume fraction, and defects. The effect of these structural attributes on the onset, propagation, and coalescence of cracks is explored. The simulation results show that spatial heterogeneity and material anisotropy highly affect crack patterns and effective fracture toughness, and the elastic contrast of two constituents significantly alters the effective toughness. However, the complex crack patterns observed in the experiments cannot completely be accounted for by either an isotropic or transversely isotropic effective medium approach. This implies that cracks developed in the layered system may coalesce in complicated ways depending on the local heterogeneity, and the interaction mechanisms between the cracks using two-constituent systems may explain the wide range of effective toughness of shale reported in the literature.

A series of constant mean stress (CMS) and constant shear stress (CSS) tests were performed to investigate the evolution of permeability and Biot coefficient at high mean stresses in a high porosity reservoir analog (Castlegate sandstone). Permeability decreases as expected with increasing mean stress, from about 20 Darcy at the beginning of the tests to between 1.5 and 0.3 Darcy at the end of the tests (mean stresses up to 275 MPa). The application of shear stress causes permeability to drop below that of a hydrostatic test at the same mean stress. Results show a nearly constant rate decrease in the Biot coefficient as the mean stress increases during hydrostatic loading, and as the shear stress increases during CMS loading. CSS tests show a stabilization of the Biot coefficient after the application of shear stress.

Abstract not provided.

A series of tests have been performed on Sierra White granite subjected to general (true triaxial) states of stress. Tests were performed under constant Lode angle conditions at Lode angles of 23.4, 16.1 and 0°. The constant Lode angle condition was maintained by holding the minimum principal stress constant while increasing the maximum and intermediate principal stress at a predetermined ratio. Tests were performed at minimum principal stresses of 5, 17 and 30 MPa. All of the specimens failed in a brittle manner, with significant dilatant volume strain accumulated, and failure showed a strong dependence on Lode angle. Specimens behaved in a nearly linear elastic manner until approximately 75% of the peak stress was reached. The angle of the failure feature (shear band) was compared to predictions developed by using the Rudnicki and Rice (1975) localization criterion. It was found that there was good agreement (within 7°) between the experimental results and theoretical predictions.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

The present study results are focused on laboratory testing of surrogate materials representing Waste Isolation Pilot Plant (WIPP) waste. The surrogate wastes correspond to a conservative estimate of the containers and transuranic waste materials emplaced at the WIPP. Testing consists of hydrostatic, triaxial, and uniaxial tests performed on surrogate waste recipes based on those previously developed by Hansen et al. (1997). These recipes represent actual waste by weight percent of each constituent and total density. Testing was performed on full-scale and 1/4-scale containers. Axial, lateral, and volumetric strain and axial and lateral stress measurements were made. Unique testing techniques were developed during the course of the experimental program. The first involves the use of a spirometer or precision flow meter to measure sample volumetric strain under the various stress conditions. Since the manner in which the waste containers deformed when compressed was not even, the volumetric and axial strains were used to determine the lateral strains. The second technique involved the development of unique coating procedures that also acted as jackets during hydrostatic, triaxial, and full-scale uniaxial testing; 1/4-scale uniaxial tests were not coated but wrapped with clay to maintain an airtight seal for volumetric strain measurement. During all testing methods, the coatings allowed the use of either a spirometer or precision flow meter to estimate the amount of air driven from the container as it crushed down since the jacket adhered to the container and yet was flexible enough to remain airtight during deformation.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

A laboratory testing program was developed to examine the short-term mechanical and time-dependent (creep) behavior of salt from the Bayou Choctaw Salt Dome. Core was tested under creep and quasi-static constant mean stress axisymmetric compression, and constant mean stress axisymmetric extension conditions. Creep tests were performed at 38 degrees Celsius, and the axisymmetric tests were performed at ambient temperatures (22-26 degrees Celsius). The testing performed indicates that the dilation criterion is pressure and stress state dependent. It was found that as the mean stress increases, the shear stress required to cause dilation increases. The results for this salt are reasonably consistent with those observed for other domal salts. Also it was observed that tests performed under extensile conditions required consistently lower shear stress to cause dilation for the same mean stress, which is consistent with other domal salts. Young's modulus ranged from 27.2 to 58.7 GPa with an average of 44.4 GPa, with Poisson's ratio ranging from 0.10 to 0.43 with an average of 0.30. Creep testing indicates that the BC salt is intermediate in creep resistance when compared with other bedded and domal salt steady-state behavior.

Abstract not provided.

Abstract not provided.

Abstract not provided.

A laboratory testing program was developed to examine the short-term mechanical and time-dependent (creep) behavior of salt from the Bayou Choctaw Salt Dome. This report documents the test methodologies, and constitutive properties inferred from tests performed. These are used to extend our understanding of the mechanical behavior of the Bayou Choctaw domal salt and provide a data set for numerical analyses. The resulting information will be used to support numerical analyses of the current state of the Bayou Choctaw Dome as it relates to its crude oil storage function as part of the US Strategic Petroleum Reserve. Core obtained from Drill Hole BC-102B was tested under creep and quasi-static constant mean stress axisymmetric compression, and constant mean stress axisymmetric extension conditions. Creep tests were performed at 100 degrees Fahrenheit, and the axisymmetric tests were performed at ambient temperatures (72-78 degrees Fahrenheit). The testing performed indicates that the dilation criterion is pressure and stress state dependent. It was found that as the mean stress increases, the shear stress required to cause dilation increases. The results for this salt are reasonably consistent with those observed for other domal salts. Also it was observed that tests performed under extensile conditions required consistently lower shear stress to cause dilation for the same mean stress, which is consistent with other domal salts. Young's moduli ranged from 3.95 x 10⁶ to 8.51 x 10⁶ psi with an average of 6.44 x 10⁶ psi, with Poisson's ratios ranging from 0.10 to 0.43 with an average of 0.30. Creep testing indicates that the BC salt is intermediate in creep resistance when compared with other bedded and domal salt steady-state behavior.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.