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III-antimonide/nitride based semiconductors for optoelectronic materials and device studies : LDRD 26518 final report

Peake, Gregory M.; Peake, Gregory M.; Klem, John F.; Modine, N.A.; Waldrip, Karen E.; Kurtz, S.R.; Allerman, A.A.; Jones, E.D.

The goal of this LDRD was to investigate III-antimonide/nitride based materials for unique semiconductor properties and applications. Previous to this study, lack of basic information concerning these alloys restricted their use in semiconductor devices. Long wavelength emission on GaAs substrates is of critical importance to telecommunication applications for cost reduction and integration into microsystems. Currently InGaAsN, on a GaAs substrate, is being commercially pursued for the important 1.3 micrometer dispersion minima of silica-glass optical fiber; due, in large part, to previous research at Sandia National Laboratories. However, InGaAsN has not shown great promise for 1.55 micrometer emission which is the low-loss window of single mode optical fiber used in transatlantic fiber. Other important applications for the antimonide/nitride based materials include the base junction of an HBT to reduce the operating voltage which is important for wireless communication links, and for improving the efficiency of a multijunction solar cell. We have undertaken the first comprehensive theoretical, experimental and device study of this material with promising results. Theoretical modeling has identified GaAsSbN to be a similar or potentially superior candidate to InGaAsN for long wavelength emission on GaAs. We have confirmed these predictions by producing emission out to 1.66 micrometers and have achieved edge emitting and VCSEL electroluminescence at 1.3 micrometers. We have also done the first study of the transport properties of this material including mobility, electron/hole mass, and exciton reduced mass. This study has increased the understanding of the III-antimonide/nitride materials enough to warrant consideration for all of the target device applications.

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The nature and origin of lateral composition modulations in short-period strained-layer superlattices

Materials Research Society Symposium - Proceedings

Norman, A.G.; Ahrenkiel, S.P.; Moutinho, H.R.; Ballif, C.; Aljassim, M.M.; Mascarenhas, A.; Follstaedt, D.M.; Lee, S.R.; Reno, J.L.; Jones, E.D.; Mirecki-Millunchick, J.; Twesten, R.D.

The nature and origin of lateral composition modulations in (AlAs)m(InAs)n short-period strained-layer superlattices grown by molecular beam epitaxy on InP substrates have been investigated by x-ray diffraction, atomic force microscopy, and transmission electron microscopy. Strong modulations were observed for growth temperatures between ~ 540 and 560° C. The maximum strength of modulations was found for SPS samples with InAs mole fraction x (= n/(n+m)) close to = 0.50 and when n - m = 2. The modulations were suppressed at both high and low values of x. For x > 0.52 (global compression), the modulations were along the <100> directions in the (001) growth plane. For x < 0.52 (global tension), the modulations were along the two <310> directions rotated = +27° from [110] in the growth plane. The remarkably constant wavelength of the modulations, between = 20-30 nm, and the different modulation directions observed, suggest that the origin of the modulations is due to surface roughening associated with the high misfit between the individual SPS layers and the InP substrate. Highly uniform unidirectional modulations have been grown by control of the InAs mole fraction and growth on suitably offcut substrates, which show great promise for application in device structures. ©2000 Materials Research Society.

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Optical properties of spontaneous lateral composition modulation in AlAs/InAs short-period superlattices

Applied Physics Letters

Francoeur, S.; Zhang, Yong; Norman, A.G.; Alsina, F.; Mascarenhas, A.; Reno, J.L.; Jones, E.D.; Lee, S.R.; Follstaedt, D.M.

The effect of lateral composition modulation, spontaneously generated during the epitaxial growth of an AlAs/InAs short-period superlattice, on the electronic band structure is investigated using phototransmission and photoluminescence spectroscopy. Compared with uniform layers of identical average composition, the presence of the composition modulation considerably reduces the band-gap energy and produces strongly polarized emission and absorption spectra. We demonstrate that the dominant polarization direction can selectively be aligned along the [1̄10] or [010] crystallographic directions. In compressively strained samples, the use of (001) InP substrates slightly miscut toward (111)A or (101) resulted in modulation directions along [110] or [100], respectively, and dominant polarization directions along a direction orthogonal to the respective composition modulation. Band-gap reductions as high as 350 and 310 meV are obtained for samples with composition modulation along [110] and [100], respectively. Ratios of polarized intensities up to 26 are observed in transmission spectra. © 2000 American Institute of Physics.

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Effect of surface steps on the microstructure of lateral composition modulation

Applied Physics Letters

Follstaedt, D.M.; Reno, J.L.; Jones, E.D.; Lee, S.R.; Norman, A.G.; Moutinho, H.R.; Mascarenhas, A.; Twesten, R.D.

Growth of InAs/AlAs short-period superlattices on appropriately miscut (001) InP substrates is shown to alter the microstructure of composition modulation from a two-dimensional organization of short compositionally enriched wires to a single dominant modulation direction with wire lengths up to ∼ 1 μm. The effects of miscut are interpreted in terms of surface step orientation and character. The material is strongly modulated and exhibits intense optical emission. The one-dimensional modulations appear potentially useful for new devices that take advantage of the preferred direction formed in the growth plane. © 2000 American Institute of Physics.

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Double Barrier Resonant Tunneling Transistor with a Fully Two Dimensional Emitter

Science Magazine

Simmons, J.A.; Reno, J.L.; Baca, Wes E.; Hietala, Vincent M.; Jones, E.D.; Simmons, J.A.

A novel planar resonant tunneling transistor is demonstrated. The growth structure is similar to that of a double-barrier resonant tunneling diode (RTD), except for a fully two-dimensional (2D) emitter formed by a quantum well. Current is fed laterally into the emitter, and the 2D--2D resonant tunneling current is controlled by a surface gate. This unique device structure achieves figures-of-merit, i.e. peak current densities and peak voltages, approaching that of state-of-the-art RTDs. Most importantly, sensitive control of the peak current and voltage is achieved by gating of the emitter quantum well subband energy. This quantum tunneling transistor shows exceptional promise for ultra-high speed and multifunctional operation at room temperature.

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GaInNAs laser gain

Chow, Weng W.; Jones, E.D.; Modine, N.A.; Kurtz, S.R.; Allerman, A.A.

The optical gain spectra for GaInNAs/GaAs quantum wells are computed using a microscopic laser theory. From these spectra, the peak gain and carrier radiative decay rate as functions of carrier density are determined. These dependences allow the study of the lasing threshold current density of GaInNAs/GaAs quantum well structures.

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The unusual conduction band minimum formation of Ga(As{sub 0.5{minus}y}P{sub 0.5{minus}y}N{sub 2y}) alloys

Physical Review Letters

Modine, N.A.; Jones, E.D.; Modine, N.A.

The conduction band minimum formation of GaAs{sub 0.5{minus}y}P{sub 0.5{minus}y}N{sub 2y} is investigated for small nitrogen compositions (0.1% < 2y < 1.0%), by using a pseudopotential technique. This formation is caused by two unusual processes both involving the deep-gap impurity level existing in the dilute alloy limit y {r_arrow} 0. The first process is an anticrossing with the {Gamma}{sub Ic}-like extended state of GaAs{sub 0.5}P{sub 0.5}. The second process is an interaction with other impurity levels forming a subband. These two processes are expected to occur in any alloys exhibiting a deep-gap impurity level at one of its dilute limit.

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Minority carrier diffusion, defects, and localization in InGaAsN with 2% nitrogen

Applied Physics Letters

Kurtz, S.R.; Allerman, A.A.; Seager, Carleton H.; Jones, E.D.

Electron and hole transport in compensated, InGaAsN ({approx} 2% N) are examined through Hall mobility, photoconductivity, and solar cell photoresponse measurements. Short minority carrier diffusion lengths, photoconductive-response spectra, and doping dependent, thermally activated Hall mobilities reveal a broad distribution of localized states. At this stage of development, lateral carrier transport appears to be limited by large scale (>> mean free path) material inhomogeneities, not a random alloy-induced mobility edge.

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Photoluminescence-linewidth-derived exciton mass for InGaAsN alloys

Physical Review B

Jones, E.D.; Allerman, A.A.; Kurtz, S.R.; Modine, N.A.

The authors report a measurement of the variation of the value of the linewidth of an excitonic transition in InGaAsN alloys (1 and 2% nitrogen) as a function of hydrostatic pressure using photoluminescence spectroscopy. The samples were grown by metal-organic chemical vapor deposition and the photoluminescence measurements were performed a 4K. The authors find that the value of the excitonic linewidth increases as a function of pressure until about 100 kbars after which it tends to saturate. This change in the excitonic linewidth is used to derive the pressure variation of the reduced mass of the exciton using a theoretical formalism which is based on the premise that the broadening of the excitonic transition is caused primarily by compositional fluctuations in a completely disordered alloy. The variation of the excitonic reduced mass thus derived is compared with that recently determined using a first-principles band structure calculation based on local density approximation.

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Reciprocal-space and real-space analyses of compositional modulation in InAs/AlAs short-period superlattices

Follstaedt, D.M.; Reno, J.L.; Jones, E.D.

The microstructure of lateral composition modulation in InAs/AlAs superlattices grown by MBE on InP is examined. The use of x-ray diffraction, TEM, AFM, and STEM to characterize the modulations is discussed. Combining the information from these techniques gives increased insight into the phenomenon and how to manipulate it. Diffraction measures the intensity of modulation and its wavelength, and is used to identify growth conditions giving strong modulation. The TEM and STEM analyses indicate that local compositions are modulated by as much as 0.38 InAs mole fraction. Plan-view images show that modulated structures consists of short ({approx_lt}0.2 {micro}m) In-rich wires with a 2D organization in a (001) growth plane. However, growth on miscut substrates can produce a single modulation along the miscut direction with much longer wires ({approx_gt}0.4 {micro}m), as desired for potential applications. Photoluminescence studies demonstrate that the modulation has large effects on the bandgap energy of the superlattice.

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Effective masses for small nitrogen concentrations in InGaAsN alloys on GaAs

Proceedings of SPIE - The International Society for Optical Engineering

Jones, E.D.; Allerman, A.A.; Kurtz, S.R.; Fritz, I.J.; Modine, N.A.; Sieg, R.M.; Bajaj, K.K.; Tozer, S.W.; Wei, X.

The variation of the value of the linewidth of an excitonic transition in InGaAsN alloys (1% and 2% nitrogen) as a function of hydrostatic pressure using photoluminescence spectroscopy is studied at 4 K. The excitonic linewidth increases as a function of pressure until about 100 kbar after which it tends to saturate. This pressure dependent excitonic linewidth is used to derive the pressure variation of the exciton reduced mass using a theoretical formalism based on the premise that the broadening of the excitonic transition is caused primarily by compositional fluctuations in a completely disordered alloy. The linewidth derived ambient pressure masses are compared and found to be in agreement with other mass measurements. The variation of this derived mass is compared with the results from a nearly first-principles approach in which calculations based on the local density approximation to the Kohn-Sham density functional theory are corrected using a small amount of experimental input.

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13 Results
13 Results