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Cascaded Optical Nonlinearities in Dielectric Metasurfaces

ACS Photonics

Gennaro, Sylvain D.; Doiron, Chloe F.; Karl, Nicholas J.; Padmanabha Iyer, Prasad P.; Serkland, Darwin K.; Sinclair, Michael B.; Brener, Igal B.

Since the discovery of the laser, optical nonlinearities have been at the core of efficient light conversion sources. Typically, thick transparent crystals or quasi-phase matched waveguides are utilized in conjunction with phase-matching techniques to select a single parametric process. In recent years, due to the rapid developments in artificially structured materials, optical frequency mixing has been achieved at the nanoscale in subwavelength resonators arrayed as metasurfaces. Phase matching becomes relaxed for these wavelength-scale structures, and all allowed nonlinear processes can, in principle, occur on an equal footing. This could promote harmonic generation via a cascaded (consisting of several frequency mixing steps) process. However, so far, all reported work on dielectric metasurfaces have assumed frequency mixing from a direct (single step) nonlinear process. In this work, we prove the existence of cascaded second-order optical nonlinearities by analyzing the second- and third-wave mixing from a highly nonlinear metasurface in conjunction with polarization selection rules and crystal symmetries. We find that the third-wave mixing signal from a cascaded process can be of comparable strength to that from conventional third-harmonic generation and that surface nonlinearities are the dominant mechanism that contributes to cascaded second-order nonlinearities in our metasurface.

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Silicon Consortium Project: No-Go on Moir Interferometry for Measuring SEI Strain as a Probe for Calendar Life Testing

McBrayer, Josefine D.; Serkland, Darwin K.; Fenton, Kyle R.; Apblett, Christopher A.; Minteer, Shelley D.; Harrison, Katharine L.

Silicon is a promising candidate as a next generation anode to replace or complement graphite electrodes due to its high energy density and low lithiation potential. When silicon is lithiated, it experiences over 300% expansion which stresses the silicon as well as its solid electrolyte interphase (SEI) leading to poor performance. The use of nano-sized silicon has helped to mitigate volume expansion and stress in the silicon, yet the silicon SEI is still both mechanically and chemically unstable. Identifying the mechanical failure mechanism of the SEI will help enhance calendar and cycle life performance through improved SEI design. In situ moiré interferometry was investigated to try and track the in-plane strain in the SEI and silicon electrode for this purpose. Moiré can detect on the order of 10 nm changes in displacement and is therefore a useful tool in the measurement of strain. As the sample undergoes small deformations, large changes in the moiré fringe allow for measurements of displacement below the diffraction limit of light. Figure 1a shows how the moiré fringe changes as the sample grating deforms. As the sample contracts or expands, the frequency of the moiré fringe changes, and this change is proportional to the strain in the sample.

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Analyzing Custom Proof Masses and Quantum Limits of a Manufacturable Cavity Optical Levitation Solution

Grine, Alejandro J.; Serkland, Darwin K.; Schultz, Justin S.; Wood, Michael G.; Finnegan, Patrick S.; Weatherred, Scott E.; Peake, Gregory M.; Sandoval, Annette S.; Alliman, Darrel A.; Li, Tongcang L.; Seberson, Troy S.

This report details results of a one-year LDRD to understand the dynamics, figures of merit, and fabrication possibilities for levitating a micro-scale, disk-shaped dielectric in an optical field. Important metrics are the stability, positional uncertainty, and required optical power to maintain levitation. Much of the results are contained in a publication written by our academic alliance collaborators. Initial structures were grown at Sandia labs and a test fabrication flow was executed. Owing to our strength in VCSEL lasers, we were particularly interested in calculations and fabrication flows that could be compatible with a VCSEL light source.

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Optically-triggered optical limiters for short-wavelength infrared sensor protection

Optics InfoBase Conference Papers

Wood, Michael G.; McKay, Alec; Morin, Theodore J.; Serkland, Darwin K.; Luk, Ting S.; Wolfley, Steven L.; Gastian, Loren G.; Mudrick, John M.; Jasperson, Ben; Johnson, Harley T.

We report experimental and numerical developments extending the operating range of vanadium dioxide based optical limiters into the short-wavelength infrared. Pixelated sensor elements have been fabricated which show optically-triggered limiting of a 2.7 µm probe.

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Heterogeneous Integration of Silicon Electronics and Compound Semiconductor Optoelectronics for Miniature RF Photonic Transceivers

Nordquist, Christopher N.; Skogen, Erik J.; Fortuna, S.A.; Hollowell, Andrew E.; Hemmady, Caroline S.; Saugen, J.M.; Forbes, T.; Wood, Michael G.; Jordan, Matthew J.; McClain, Jaime L.; Lepkowski, Stefan M.; Alford, Charles A.; Peake, Gregory M.; Pomerene, Andrew P.; Long, Christopher M.; Serkland, Darwin K.; Dean, Kenneth A.

Abstract not provided.

Heterogeneous integration of silicon electronics and compound semiconductor optoelectronics for miniature rf photonic transceivers

ECS Transactions

Nordquist, C.D.; Skogen, Erik J.; Fortuna, S.A.; Hollowell, Andrew E.; Hemmady, C.S.; Saugen, J.M.; Forbes, T.; Wood, M.G.; Jordan, Matthew J.; McClain, Jaime L.; Lepkowski, Stefan M.; Alford, Charles A.; Peake, Gregory M.; Pomerene, Andrew P.; Long, C.M.; Serkland, Darwin K.; Dean, Kenneth A.

Heterogeneous Integration (HI) may enable optoelectronic transceivers for short-range and long-range radio frequency (RF) photonic interconnect using wavelength-division multiplexing (WDM) to aggregate signals, provide galvanic isolation, and reduce crosstalk and interference. Integration of silicon Complementary Metal-Oxide-Semiconductor (CMOS) electronics with InGaAsP compound semiconductor photonics provides the potential for high-performance microsystems that combine complex electronic functions with optoelectronic capabilities from rich bandgap engineering opportunities, and intimate integration allows short interconnects for lower power and latency. The dominant pure-play foundry model plus the differences in materials and processes between these technologies dictate separate fabrication of the devices followed by integration of individual die, presenting unique challenges in die preparation, metallization, and bumping, especially as interconnect densities increase. In this paper, we describe progress towards realizing an S-band WDM RF photonic link combining 180 nm silicon CMOS electronics with InGaAsP integrated optoelectronics, using HI processes and approaches that scale into microwave and millimeter-wave frequencies.

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High-mobility transparent conducting oxides for compact epsilon-near-zero silicon photonic phase modulators

Optics InfoBase Conference Papers

Wood, Michael G.; Reines, Isak C.; Luk, Ting S.; Serkland, Darwin K.; Campione, Salvatore

We numerically analyze the role of carrier mobility in transparent conducting oxides in epsilon-near-zero phase modulators. High-mobility materials such as cadmium oxide enable compact photonic phase modulators with a modulation figure of merit >29 º/dB.

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All-Semiconductor Coupled-Cavity VCSELs for Narrow Linewidth

Conference Digest - IEEE International Semiconductor Laser Conference

Serkland, Darwin K.; Morin, Theodore J.; Grine, Alejandro J.; Peake, Gregory M.; Kendall, Wesley Y.; Wood, Michael G.; Hains, Christopher H.; So, Haley M.; Soudachanh, Amy L.; Geib, Kent M.

We demonstrate an all-semiconductor coupled-cavity VCSEL designed to achieve narrow linewidth at 850 nm. A resonant AlGaAs cavity of thickness 1,937 nm (8 wavelengths) is situated below the 3-quantum-well active region and results in an effective coupled-cavity length of 36 wavelengths.

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Compact epsilon-near-zero silicon photonic phase modulators

Optics Express

Reines, Isak C.; Wood, Michael G.; Luk, Ting S.; Serkland, Darwin K.; Campione, Salvatore

In this paper, we analyze a compact silicon photonic phase modulator at 1.55 μm using epsilon-near-zero transparent conducting oxide (TCO) films. The operating principle of the non-resonant phase modulator is field-effect carrier density modulation in a thin TCO film deposited on top of a passive silicon waveguide with a CMOS-compatible fabrication process. We compare phase modulator performance using both indium oxide (In2O3) and cadmium oxide (CdO) TCO materials. Our findings show that practical phase modulation can be achieved only when using high-mobility (i.e. low-loss) epsilon-near-zero materials such as CdO. The CdO-based phase modulator has a figure of merit of 17.1°/dB in a compact 5 μm length. This figure of merit can be increased further through the proper selection of high-mobility TCOs, opening a path for device miniaturization and increased phase shifts.

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Frequency Noise of Silicon Nitride Optomechanical Oscillators with Integrated Waveguides

Grine, Alejandro J.; Grine, Alejandro J.; Serkland, Darwin K.; Serkland, Darwin K.; Wood, Michael G.; Wood, Michael G.; Soudachanh, Amy L.; Soudachanh, Amy L.; Hollowell, Andrew E.; Hollowell, Andrew E.; Koch, Lawrence K.; Koch, Lawrence K.; Hains, Christopher H.; Hains, Christopher H.; Siddiqui, Aleem M.; Siddiqui, Aleem M.; Eichenfield, Matthew S.; Eichenfield, Matthew S.; Dagel, Daryl D.; Dagel, Daryl D.; Grossetete, Grant G.; Grossetete, Grant G.; Matins, Benjamin M.; Matins, Benjamin M.

Abstract not provided.

Gigahertz speed operation of epsilon-near-zero silicon photonic modulators

Optica

Wood, Michael G.; Campione, Salvatore; Parameswaran, S.; Luk, Ting S.; Wendt, J.R.; Serkland, Darwin K.; Keeler, Gordon A.

Optical communication systems increasingly require electrooptical modulators that deliver high modulation speeds across a large optical bandwidth with a small device footprint and a CMOS-compatible fabrication process. Although silicon photonic modulators based on transparent conducting oxides (TCOs) have shown promise for delivering on these requirements, modulation speeds to date have been limited. Here, we describe the design, fabrication, and performance of a fast, compact electroabsorption modulator based on TCOs. The modulator works by using bias voltage to increase the carrier density in the conducting oxide, which changes the permittivity and hence optical attenuation by almost 10 dB. Under bias, light is tightly confined to the conducting oxide layer through nonresonant epsilon-near-zero (ENZ) effects, which enable modulation over a broad range of wavelengths in the telecommunications band. Our approach features simple integration with passive silicon waveguides, the use of stable inorganic materials, and the ability to modulate both transverse electric and magnetic polarizations with the same device design. Using a 4-μm-long modulator and a drive voltage of 2 Vpp, we demonstrate digital modulation at rates of 2.5 Gb/s. We report broadband operation with a 6.5 dB extinction ratio across the 1530–1590 nm band and a 10 dB insertion loss. This work verifies that high-speed ENZ devices can be created using conducting oxide materials and paves the way for additional technology development that could have a broad impact on future optical communications systems.

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Mode selection and tuning of single-frequency short-cavity VECSELs

Proceedings of SPIE - The International Society for Optical Engineering

Serkland, Darwin K.; So, Haley M.; Peake, Gregory M.; Wood, Michael G.; Grine, Alejandro J.; Hains, Christopher H.; Geib, Kent M.; Keeler, Gordon A.

We report on mode selection and tuning properties of vertical-external-cavity surface-emitting lasers (VECSELs) containing coupled semiconductor and external cavities of total length less than 1 mm. Our goal is to create narrowlinewidth (<1MHz) single-frequency VECSELs that operate near 850 nm on a single longitudinal cavity resonance and tune versus temperature without mode hops. We have designed, fabricated, and measured VECSELs with external-cavity lengths ranging from 25 to 800 μm. We compare simulated and measured coupled-cavity mode frequencies and discuss criteria for single mode selection.

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Optomechanical spring effect readout in resonant micro-optical Sagnac gyroscopes design and scaling analysis

International Conference on Optical MEMS and Nanophotonics

Grine, Alejandro J.; Siddiqui, A.; Keeler, Gordon A.; Shaw, M.J.; Eichenfield, Matthew S.; Friedmann, Thomas A.; Douglas, Erica A.; Wood, M.G.; Dagel, D.J.; Hains, C.; Koch, L.F.; Nordquist, C.D.; Serkland, Darwin K.

We propose and theoretically analyze a new cavity optomechanical oscillator gyroscope. Mechanical frequency acts as a sensitive readout of rotation through the optomechanical spring and Sagnac effects. Remarkably, reducing device size improves scale factor.

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Submicrometer Epsilon-Near-Zero Electroabsorption Modulators Enabled by High-Mobility Cadmium Oxide

IEEE Photonics Journal

Campione, Salvatore; Wood, Michael G.; Serkland, Darwin K.; Parameswaran, Sivasubramanian P.; Ihlefeld, Jon I.; Luk, Ting S.; Wendt, J.R.; Geib, Kent M.; Keeler, Gordon A.

Epsilon-near-zero materials provide a new path for tailoring light-matter interactions at the nanoscale. In this paper, we analyze a compact electroabsorption modulator based on epsilon-near-zero confinement in transparent conducting oxide films. The nonresonant modulator operates through field-effect carrier density tuning. We compare the performance of modulators composed of two different conducting oxides, namely, indium oxide (In2O3) and cadmium oxide (CdO), and show that better modulation performance is achieved when using high-mobility (i.e., low loss) epsilon-near-zero materials such as CdO. In particular, we show that nonresonant electroabsorption modulators with submicron lengths and greater than 5 dB extinction ratios may be achieved through the proper selection of high-mobility transparent conducting oxides, opening a path for device miniaturization and increased modulation depth.

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Modeling charge collection efficiency degradation in partially depleted GaAs photodiodes using the 1- and 2-carrier Hecht equations

Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms

Auden, E.C.; Vizkelethy, Gyorgy V.; Serkland, Darwin K.; Bossert, David B.; Doyle, Barney L.

The Hecht equation can be used to model the nonlinear degradation of charge collection efficiency (CCE) in response to radiation-induced displacement damage in both fully and partially depleted GaAs photodiodes. CCE degradation is measured for laser-generated photocurrent as a function of fluence and bias in Al0.3Ga0.7As/GaAs/Al0.25Ga0.75As p-i-n photodiodes which have been irradiated with 12 MeV C and 7.5 MeV Si ions. CCE is observed to degrade more rapidly with fluence in partially depleted photodiodes than in fully depleted photodiodes. When the intrinsic GaAs layer is fully depleted, the 2-carrier Hecht equation describes CCE degradation as photogenerated electrons and holes recombine at defect sites created by radiation damage in the depletion region. If the GaAs layer is partially depleted, CCE degradation is more appropriately modeled as the sum of the 2-carrier Hecht equation applied to electrons and holes generated within the depletion region and the 1-carrier Hecht equation applied to minority carriers that diffuse from the field-free (non-depleted) region into the depletion region. Enhanced CCE degradation is attributed to holes that recombine within the field-free region of the partially depleted intrinsic GaAs layer before they can diffuse into the depletion region.

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High-mobility transparent conducting oxides for compact epsilon-near-zero silicon integrated optical modulators

Optics InfoBase Conference Papers

Wood, Michael G.; Campione, Salvatore; Serkland, Darwin K.; Parameswaran, Sivasubramanian P.; Ihlefeld, Jon; Luk, Ting S.; Wendt, J.R.; Geib, Kent M.; Keeler, Gordon A.

We study the role of carrier mobility in transparent conducting oxides integrated into epsilon-near-zero modulators. High-mobility materials including CdO enable sub-micron length electroabsorption modulators through >4dB/μm extinction ratios.

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VCSELs for interferometric readout of MEMS sensors

Proceedings of SPIE - The International Society for Optical Engineering

Serkland, Darwin K.; Geib, K.M.; Peake, Gregory M.; Keeler, Gordon A.; Shaw, Michael S.; Baker, Michael S.; Okandan, Murat

We report on the development of single-frequency VCSELs (vertical-cavity surface-emitting lasers) for sensing the position of a moving MEMS (micro-electro-mechanical system) object with resolution much less than 1nm. Position measurement is the basis of many different types of MEMS sensors, including accelerometers, gyroscopes, and pressure sensors. Typically, by switching from a traditional capacitive electronic readout to an interferometric optical readout, the resolution can be improved by an order of magnitude with a corresponding improvement in MEMS sensor performance. Because the VCSEL wavelength determines the scale of the position measurement, laser wavelength (frequency) stability is desirable. This paper discusses the impact of VCSEL amplitude and frequency noise on the position measurement.

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Final report on LDRD project : narrow-linewidth VCSELs for atomic microsystems

Serkland, Darwin K.; Chow, Weng W.; Geib, K.M.; Peake, Gregory M.

Vertical-cavity surface-emitting lasers (VCSELs) are well suited for emerging photonic microsystems due to their low power consumption, ease of integration with other optical components, and single frequency operation. However, the typical VCSEL linewidth of 100 MHz is approximately ten times wider than the natural linewidth of atoms used in atomic beam clocks and trapped atom research, which degrades or completely destroys performance in those systems. This report documents our efforts to reduce VCSEL linewidths below 10 MHz to meet the needs of advanced sub-Doppler atomic microsystems, such as cold-atom traps. We have investigated two complementary approaches to reduce VCSEL linewidth: (A) increasing the laser-cavity quality factor, and (B) decreasing the linewidth enhancement factor (alpha) of the optical gain medium. We have developed two new VCSEL devices that achieved increased cavity quality factors: (1) all-semiconductor extended-cavity VCSELs, and (2) micro-external-cavity surface-emitting lasers (MECSELs). These new VCSEL devices have demonstrated linewidths below 10 MHz, and linewidths below 1 MHz seem feasible with further optimization.

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Feedback in close-coupled axial VCSEL-photodiode pairs

Proceedings of SPIE - The International Society for Optical Engineering

Geib, Kent M.; Serkland, Darwin K.; Peake, Gregory M.; Sanchez, Victoria M.

We have been investigating the use of coaxial multimode VCSEL/PD (vertical cavity surface emitting laser/photodiode) pairs for positional sensing with emitter to target mirror distances on the order of 1mm. We have observed large variations in signal levels due to the strong optical feedback in these close-coupled systems, employing either heterogeneously integrated commercial components or our own monolithically integrated devices. The feedback effect is larger than anticipated due to the annular geometry of the photodetector. Even though there is very little change in the measured VCSEL total output power, the optical feedback induces variations in the transverse mode distributions in these multimode VCSELs. The higher order modes have a larger divergence angle resulting in changes in the reflected light power incident upon the active detector area for a large range of emitter/mirror separations. We will review the experimental details and provide strategies for avoiding these variations in detected power. © 2011 Copyright Society of Photo-Optical Instrumentation Engineers (SPIE).

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High-speed reflective S-SEEDs for photonic logic circuits

2009 International Conference on Photonics in Switching, PS '09

Keeler, Gordon A.; Serkland, Darwin K.; Overberg, Mark E.; Geib, K.M.; Gill, D.D.; Mukherjee, Sayan M.; Hsu, Alan Y.; Clevenger, Jascinda C.; Baiocchi, D.; Sweatt, W.C.

We demonstrate the operation of low-power reflective S-SEEDs with 6-ps switching times at a 2-Volt bias. Efficient refractive micro-optics are used to optically interconnect multiple S-SEED gates. The technology platform is expected to enable dense photonic logic circuits for high-speed telecommunications-related applications. © 2009 IEEE.

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Growth, fabrication, and characterization of high-speed 1550-nm S-SEEDs for all-optical logic

ECS Transactions

Keeler, Gordon A.; Serkland, Darwin K.; Overberg, Mark E.; Klem, John F.; Geib, K.M.; Clevenger, Jascinda C.; Hsu, Alan Y.; Hadley, G.R.

We describe recent advances in the development of 1550-nm symmetric self-electrooptic effect devices (S-SEEDs). S-SEEDs are semiconductor optoelectronic devices used to implement ultrafast all-optical logic functions: for optical fiber communication applications. In this paper, basic S-SEED operation is described, followed by a detailed explanation of the optimization techniques used to improve DC and high-speed performance in these long wavelength devices. Both epitaxial strain and quantum well design are shown to be important for S-SEEDs grown in the InAlGaAs quaternary material system. The device fabrication approach is outlined, and DC electrical and optical performance is discussed. Finally, we describe the high-speed optoelectronic measurements used to determine S-SEED switching characteristics. The devices described herein are the first known S-SEEDs to operate at telecommunications- compatible wavelengths and demonstrate record switching speeds with rail-to-rail switching rates faster than 6 picoseconds. © The Electrochemical Society.

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17 G directly modulated datacom VCSELs

2008 Conference on Quantum Electronics and Laser Science Conference on Lasers and Electro-Optics, CLEO/QELS

Johnson, Ralph H.; Serkland, Darwin K.

The next generation 850 nm datacom VCSEL to go into production will be the 17 G VCSEL. It is not certain that direct modulation will be suitable given the reliability, supply voltage, and temperature range required. This paper is a first look at VCSELs designed and targeted for production 17 G use. The design is discussed and LIV and small signal frequency response is presented. © 2008 Optical Society of America.

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Final report on LDRD project : advanced optical trigger systems

Serkland, Darwin K.; Mar, Alan M.; Geib, K.M.; Peake, Gregory M.; Roose, Lars D.; Keeler, Gordon A.; Hadley, G.R.; Loubriel, Guillermo M.; Sullivan, Charles T.

Advanced optically-activated solid-state electrical switch development at Sandia has demonstrated multi-kA/kV switching and the path for scalability to even higher current/power. Realization of this potential requires development of new optical sources/switches based on key Sandia photonic device technologies: vertical-cavity surface-emitting lasers (VCSELs) and photoconductive semiconductor switch (PCSS) devices. The key to increasing the switching capacity of PCSS devices to 5kV/5kA and higher is to distribute the current in multiple parallel line filaments triggered by an array of high-brightness line-shaped illuminators. Commercial mechanically-stacked edge-emitting lasers have been used to trigger multiple filaments, but they are difficult to scale and manufacture with the required uniformity. In VCSEL arrays, adjacent lasers utilize identical semiconductor material and are lithographically patterned to the required dimensions. We have demonstrated multiple-line filament triggering using VCSEL arrays to approximate line generation. These arrays of uncoupled circular-aperture VCSELs have fill factors ranging from 2% to 30%. Using these arrays, we have developed a better understanding of the illumination requirements for stable triggering of multiple-filament PCSS devices. Photoconductive semiconductor switch (PCSS) devices offer advantages of high voltage operation (multi-kV), optical isolation, triggering with laser pulses that cannot occur accidentally in nature, low cost, high speed, small size, and radiation hardness. PCSS devices are candidates for an assortment of potential applications that require multi-kA switching of current. The key to increasing the switching capacity of PCSS devices to 5kV/5kA and higher is to distribute the current in multiple parallel line filaments triggered by an array of high-brightness line-shaped illuminators. Commercial mechanically-stacked edge-emitting lasers have been demonstrated to trigger multiple filaments, but they are difficult to scale and manufacture with the required uniformity. As a promising alternative to multiple discrete edge-emitting lasers, a single wafer of vertical-cavity surface-emitting lasers (VCSELs) can be lithographically patterned to achieve the desired layout of parallel line-shaped emitters, in which adjacent lasers utilize identical semiconductor material and thereby achieve a degree of intrinsic optical uniformity. Under this LDRD project, we have fabricated arrays of uncoupled circular-aperture VCSELs to approximate a line-shaped illumination pattern, achieving optical fill factors ranging from 2% to 30%. We have applied these VCSEL arrays to demonstrate single and dual parallel line-filament triggering of PCSS devices. Moreover, we have developed a better understanding of the illumination requirements for stable triggering of multiple-filament PCSS devices using VCSEL arrays. We have found that reliable triggering of multiple filaments requires matching of the turn-on time of adjacent VCSEL line-shaped-arrays to within approximately 1 ns. Additionally, we discovered that reliable triggering of PCSS devices at low voltages requires more optical power than we obtained with our first generation of VCSEL arrays. A second generation of higher-power VCSEL arrays was designed and fabricated at the end of this LDRD project, and testing with PCSS devices is currently underway (as of September 2008).

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Electronic/photonic interfaces for ultrafast data processing

Keeler, Gordon A.; Serkland, Darwin K.; Hsu, Alan Y.; Geib, K.M.; Overberg, Mark E.

This report summarizes a 3-month program that explored the potential areas of impact for electronic/photonic integration technologies, as applied to next-generation data processing systems operating within 100+ Gb/s optical networks. The study included a technology review that targeted three key functions of data processing systems, namely receive/demultiplexing/clock recovery, data processing, and transmit/multiplexing. Various technical approaches were described and evaluated. In addition, we initiated the development of high-speed photodetectors and hybrid integration processes, two key elements of an ultrafast data processor. Relevant experimental results are described herein.

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Final report on LDRD project 105967 : exploring the increase in GaAs photodiode responsivity with increased neutron fluence

Blansett, Ethan B.; Serkland, Darwin K.; Geib, K.M.; Peake, Gregory M.; Fleming, Robert M.; Wrobel, Diana L.

A previous LDRD studying radiation hardened optoelectronic components for space-based applications led to the result that increased neutron irradiation from a fast-burst reactor caused increased responsivity in GaAs photodiodes up to a total fluence of 4.4 x 10{sup 13} neutrons/cm{sup 2} (1 MeV Eq., Si). The silicon photodiodes experienced significant degradation. Scientific literature shows that neutrons can both cause defects as well as potentially remove defects in an annealing-like process in GaAs. Though there has been some modeling that suggests how fabrication and radiation-induced defects can migrate to surfaces and interfaces in GaAs and lead to an ordering effect, it is important to consider how these processes affect the performance of devices, such as the basic GaAs p-i-n photodiode. In this LDRD, we manufactured GaAs photodiodes at the MESA facility, irradiated them with electrons and neutrons at the White Sands Missile Range Linac and Fast Burst Reactor, and performed measurements to show the effect of irradiation on dark current, responsivity and high-speed bandwidth.

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Integrated NEMS and optoelectronics for sensor applications

Czaplewski, David A.; Krishnamoorthy, Uma K.; Okandan, Murat O.; Olsson, Roy H.; Serkland, Darwin K.; Warren, M.E.

This work utilized advanced engineering in several fields to find solutions to the challenges presented by the integration of MEMS/NEMS with optoelectronics to realize a compact sensor system, comprised of a microfabricated sensor, VCSEL, and photodiode. By utilizing microfabrication techniques in the realization of the MEMS/NEMS component, the VCSEL and the photodiode, the system would be small in size and require less power than a macro-sized component. The work focused on two technologies, accelerometers and microphones, leveraged from other LDRD programs. The first technology was the nano-g accelerometer using a nanophotonic motion detection system (67023). This accelerometer had measured sensitivity of approximately 10 nano-g. The Integrated NEMS and optoelectronics LDRD supported the nano-g accelerometer LDRD by providing advanced designs for the accelerometers, packaging, and a detection scheme to encapsulate the accelerometer, furthering the testing capabilities beyond bench-top tests. A fully packaged and tested die was never realized, but significant packaging issues were addressed and many resolved. The second technology supported by this work was the ultrasensitive directional microphone arrays for military operations in urban terrain and future combat systems (93518). This application utilized a diffraction-based sensing technique with different optical component placement and a different detection scheme from the nano-g accelerometer. The Integrated NEMS LDRD supported the microphone array LDRD by providing custom designs, VCSELs, and measurement techniques to accelerometers that were fabricated from the same operational principles as the microphones, but contain proof masses for acceleration transduction. These devices were packaged at the end of the work.

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Multi-filament triggering of PCSS for high current utilizing VCSEL triggers

PPPS-2007 - Pulsed Power Plasma Science 2007

Mar, Alan; Serkland, Darwin K.; Keeler, Gordon A.; Roose, Lars D.; Geib, K.M.; Loubriel, Guillermo M.; Zutavern, Fred J.

We are developing advanced optically-activated solid-state switch technology for Firing Sets. Advanced switch development at Sandia has demonstrated multikA/kV switching and the path for scalability to even higher current/power, resulting in good prospects for sprytron replacement and other even higher current pulsed power switching applications. Realization of this potential requires development of new optical sources/switches based on key Sandia photonic device technologies: vertical-cavity surface-emitting lasers (VCSELs) and photoconductive semiconductor switch (PCSS) devices. The key to increasing the switching capacity of PCSS devices to 5kV/5kA and higher has been to distribute the current in multiple parallel line filaments triggered by an array of high-brightness line-shaped illuminators.1 This was limited by commercial mechanically-stacked edgeemitting lasers, which are difficult to scale and manufacture with the required uniformity. In VCSEL arrays, adjacent lasers utilize identical semiconductor material and are lithographically patterned to the required aspect ratio. However, we have demonstrated that good optical uniformity in rectangular-aperture (e.g. 5-by- 500μmu; m) VCSELs is difficult to achieve due to the lack of optical confinement in the long dimension. We have demonstrated line filament triggering using 1-D VCSEL arrays to approximate line generation. These arrays of uncoupled circular-aperture VCSELs have fill factors ranging from 2% to 40%. Using these arrays, we are developing a better understanding of the illumination requirements for stable triggering of multiple-filament PCSS devices. In particular, we are examining the dependence of filament formation versus the illumination fill factor and spatial brightness along the length of the filament. Ultimately, we will apply effective index techniques, pioneered at Sandia for leaky-mode VCSELs, to create a lateral photonic lattice that selects a single transverse mode with high brightness and uniformity for even higher fill factors and illumination unformity.2 These sources will be developed and tested with complementary PCSS designs employing interdigitatedmulti-filament contacts for high-power switching. ©2007 IEEE.

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Final LDRD report : development of advanced UV light emitters and biological agent detection strategies

Crawford, Mary H.; Armstrong, Andrew A.; Allerman, A.A.; Figiel, J.J.; Schmitt, Randal L.; Serkland, Darwin K.

We present the results of a three year LDRD project which has focused on the development of novel, compact, ultraviolet solid-state sources and fluorescence-based sensing platforms that apply such devices to the sensing of biological and nuclear materials. We describe our development of 270-280 nm AlGaN-based semiconductor UV LEDs with performance suitable for evaluation in biosensor platforms as well as our development efforts towards the realization of a 340 nm AlGaN-based laser diode technology. We further review our sensor development efforts, including evaluation of the efficacy of using modulated LED excitation and phase sensitive detection techniques for fluorescence detection of bio molecules and uranyl-containing compounds.

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The chip-scale atomic clock : prototype evaluation

Serkland, Darwin K.; Geib, K.M.; Peake, Gregory M.

The authors have developed a chip-scale atomic clock (CSAC) for applications requiring atomic timing accuracy in portable battery-powered applications. At PTTI/FCS 2005, they reported on the demonstration of a prototype CSAC, with an overall size of 10 cm{sup 3}, power consumption > 150 mW, and short-term stability sy(t) < 1 x 10-9t-1/2. Since that report, they have completed the development of the CSAC, including provision for autonomous lock acquisition and a calibrated output at 10.0 MHz, in addition to modifications to the physics package and system architecture to improve performance and manufacturability.

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Ultrasensitive directional microphone arrays for military operations in urban terrain

Okandan, Murat O.; Parker, Eric P.; Resnick, Paul J.; Serkland, Darwin K.

Acoustic sensing systems are critical elements in detection of sniper events. The microphones developed in this project enable unique sensing systems that benefit significantly from the enhanced sensitivity and extremely compact foot-print. Surface and bulk micromachining technologies developed at Sandia have allowed the design, fabrication and characterization of these unique sensors. We have demonstrated sensitivity that is only available in 1/2 inch to 1 inch studio reference microphones--with our devices that have only 1 to 2mm diameter membranes in a volume less than 1cm{sup 3}.

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VCSEL polarization control for chip-scale atomic clocks

Keeler, Gordon A.; Geib, K.M.; Serkland, Darwin K.; Peake, Gregory M.; Wendt, J.R.

Sandia National Laboratories and Mytek, LLC have collaborated to develop a monolithically-integrated vertical-cavity surface-emitting laser (VCSEL) assembly with controllable polarization states suitable for use in chip-scale atomic clocks. During the course of this work, a robust technique to provide polarization control was modeled and demonstrated. The technique uses deeply-etched surface gratings oriented at several different rotational angles to provide VCSEL polarization stability. A rigorous coupled-wave analysis (RCWA) model was used to optimize the design for high polarization selectivity and fabrication tolerance. The new approach to VCSEL polarization control may be useful in a number of defense and commercial applications, including chip-scale atomic clocks and other low-power atomic sensors.

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Control of VCSEL polarization using deeply etched surface gratings

Conference on Lasers and Electro-Optics and 2006 Quantum Electronics and Laser Science Conference, CLEO/QELS 2006

Keeler, Gordon A.; Geib, K.M.; Serkland, Darwin K.; Peake, Gregory M.; Wendt, J.R.

We demonstrate a robust approach to VCSEL polarization control using deeply-etched surface gratings oriented at several different rotational angles. A RCWA model is used to optimize the design for high polarization selectivity and fabrication tolerance. © 2006 Optical Society of America.

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Final report on LDRD project : single-photon-sensitive imaging detector arrays at 1600 nm

Serkland, Darwin K.; Childs, Kenton D.; Koudelka, Robert K.; Geib, K.M.; Klem, John F.; Hawkins, Samuel D.; Patel, Rupal K.

The key need that this project has addressed is a short-wave infrared light detector for ranging (LIDAR) imaging at temperatures greater than 100K, as desired by nonproliferation and work for other customers. Several novel device structures to improve avalanche photodiodes (APDs) were fabricated to achieve the desired APD performance. A primary challenge to achieving high sensitivity APDs at 1550 nm is that the small band-gap materials (e.g., InGaAs or Ge) necessary to detect low-energy photons exhibit higher dark counts and higher multiplication noise compared to materials like silicon. To overcome these historical problems APDs were designed and fabricated using separate absorption and multiplication (SAM) regions. The absorption regions used (InGaAs or Ge) to leverage these materials 1550 nm sensitivity. Geiger mode detection was chosen to circumvent gain noise issues in the III-V and Ge multiplication regions, while a novel Ge/Si device was built to examine the utility of transferring photoelectrons in a silicon multiplication region. Silicon is known to have very good analog and GM multiplication properties. The proposed devices represented a high-risk for high-reward approach. Therefore one primary goal of this work was to experimentally resolve uncertainty about the novel APD structures. This work specifically examined three different designs. An InGaAs/InAlAs Geiger mode (GM) structure was proposed for the superior multiplication properties of the InAlAs. The hypothesis to be tested in this structure was whether InAlAs really presented an advantage in GM. A Ge/Si SAM was proposed representing the best possible multiplication material (i.e., silicon), however, significant uncertainty existed about both the Ge material quality and the ability to transfer photoelectrons across the Ge/Si interface. Finally a third pure germanium GM structure was proposed because bulk germanium has been reported to have better dark count properties. However, significant uncertainty existed about the quantum efficiency at 1550 nm the necessary operating temperature. This project has resulted in several conclusions after fabrication and measurement of the proposed structures. We have successfully demonstrated the Ge/Si proof-of-concept in producing high analog gain in a silicon region while absorbing in a Ge region. This has included significant Ge processing infrastructure development at Sandia. However, sensitivity is limited at low temperatures due to high dark currents that we ascribe to tunneling. This leaves remaining uncertainty about whether this structure can achieve the desired performance with further development. GM detection in InGaAs/InAlAs, Ge/Si, Si and pure Ge devices fabricated at Sandia was shown to overcome gain noise challenges, which represents critical learning that will enable Sandia to respond to future single photon detection needs. However, challenges to the operation of these devices in GM remain. The InAlAs multiplication region was not found to be significantly superior to current InP regions for GM, however, improved multiplication region design of InGaAs/InP APDs has been highlighted. For Ge GM detectors it still remains unclear whether an optimal trade-off of parameters can achieve the necessary sensitivity at 1550 nm. To further examine these remaining questions, as well as other application spaces for these technologies, funding for an Intelligence Community post-doc was awarded this year.

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In-situ optical time-domain reflectometry (OTDR) for VCSEL-based communication systems

Proceedings of SPIE - The International Society for Optical Engineering

Keeler, Gordon A.; Serkland, Darwin K.; Geib, K.M.; Klem, John F.; Peake, Gregory M.

Optical lime-domain reflectometry (OTDR) is an effeclive technique for locating faults in fiber communication links. The fact that most OTDR measurements are performed manually is a significant drawback, because it makes them too costly for use in many short-distance networks and too slow for use in military avionic platforms. Here we describe and demonstrate an automated, low-cost, real-time approach to fault monitoring that can be achieved by integrating OTDR functionality directly into VCSEL-based transceivers. This built-in test capability is straightforward to implement and relevant to both multimode and single mode networks. In-situ OTDR uses the transmitter VCSEL already present in data transceivers. Fault monitoring is performed by emitting a brief optical pulse into the fiber and then turning the VCSEL off. If a fault exists, a portion of the optical pulse returns to the transceiver after a time equal to the round-trip delay through the fiber. In multimode OTDR, the signal is detected by an integrated photodetector, while in single mode OTDR the VCSEL itself can be used as a detector. Modified driver electronics perform the measurement and analysis. We demonstrate that VCSEL-based OTDR has sufficient sensitivity to determine the location of most faults commonly seen in short-haul networks (i.e., the Fresnel reflections from improperly terminated fibers and scattering from raggedly-broken fibers). Results are described for single mode and multimode experiments, at both 850 nm and 1.3 μm. We discuss the resolution and sensitivity that have been achieved, as well as expected limitations for this novel approach to network monitoring.

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High slope efficiency measured from a composite-resonator vertical-cavity laser

IEEE Photonics Technology Letters

Grasso, D.M.; Choquette, K.D.; Serkland, Darwin K.; Peake, G.M.; Geib, K.M.

We report high differential slope of the light versus current (L-I) characteristic in excess of 400% external quantum efficiency from a monolithic dual resonator vertical-cavity surface-emitting laser. The additional optical cavity of the composite resonator can provide gain or loss to the distributed laser mode, depending on the bias conditions. We describe the factors contributing to the internal optical loss, and present a qualitative model for the L-I characteristic. With sufficient current injected into the top cavity, the composite-resonator vertical-cavity laser achieves over 6 W/A of differential slope efficiency from threshold to greater than 1 mW of output power, which may be applicable for analog optical data links. © 2006 IEEE.

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Final report on LDRD project :leaky-mode VCSELs for photonic logic circuits

Serkland, Darwin K.; Geib, K.M.; Peake, Gregory M.; Hadley, G.R.; Hargett, Terry H.; Keeler, Gordon A.; Blansett, Ethan B.; Diaz, Melissa R.; Sullivan, Charles T.

This report describes the research accomplishments achieved under the LDRD Project ''Leaky-mode VCSELs for photonic logic circuits''. Leaky-mode vertical-cavity surface-emitting lasers (VCSELs) offer new possibilities for integration of microcavity lasers to create optical microsystems. A leaky-mode VCSEL output-couples light laterally, in the plane of the semiconductor wafer, which allows the light to interact with adjacent lasers, modulators, and detectors on the same wafer. The fabrication of leaky-mode VCSELs based on effective index modification was proposed and demonstrated at Sandia in 1999 but was not adequately developed for use in applications. The aim of this LDRD has been to advance the design and fabrication of leaky-mode VCSELs to the point where initial applications can be attempted. In the first and second years of this LDRD we concentrated on overcoming previous difficulties in the epitaxial growth and fabrication of these advanced VCSELs. In the third year, we focused on applications of leaky-mode VCSELs, such as all-optical processing circuits based on gain quenching.

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Electrically-pumped 850-nm micromirror VECSELs

Progress in Biomedical Optics and Imaging - Proceedings of SPIE

Keeler, Gordon A.; Serkland, Darwin K.; Geib, K.M.; Peake, Gregory M.; Mar, Alan M.

Vertical-external-cavity surface-emitting lasers (VECSELs) combine high optical power and good beam quality in a device with surface-normal output. In this paper, we describe the design and operating characteristics of an electrically-pumped VECSEL that employs a wafer-scale fabrication process and operates at 850 nm. A curved micromirror output coupler is heterogeneously integrated with AlGaAs-based semiconductor material to form a compact and robust device. The structure relies on flip-chip bonding the processed epitaxial material to an aluminum nitride mount; this heatsink both dissipates thermal energy and permits high frequency modulation using coplanar traces that lead to the VECSEL mesa. Backside emission is employed, and laser operation at 850 nm is made possible by removing the entire GaAs substrate through selective wet etching. While substrate removal eliminates absorptive losses, it simultaneously compromises laser performance by increasing series resistance and degrading the spatial uniformity of current injection. Several aspects of the VECSEL design help to mitigate these issues, including the use of a novel current-spreading n-type distributed Bragg reflector (DBR). Additionally, VECSEL performance is improved through the use of a p-type DBR that is modified for low thermal resistance.

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Photonics technology development for optical fuzing

Geib, K.M.; Serkland, Darwin K.; Keeler, Gordon A.; Peake, Gregory M.; Mar, Alan M.

This paper describes the photonic component development, which exploits pioneering work and unique expertise at Sandia National Laboratories, ARDEC and the Army Research Laboratory by combining key optoelectronic technologies to design and demonstrate components for this fuzing application. The technologies under investigation for the optical fuze design covered in this paper are vertical cavity surface emitting lasers (VECSELs), integrated resonant cavity photodetectors (RCPD), and diffractive micro-optics. The culmination of this work will be low cost, robust, fully integrated, g-hardened components designed suitable for proximity fuzing applications. The use of advanced photonic components will enable replacement of costly assemblies that employ discrete lasers, photodetectors, and bulk optics. The integrated devices will be mass produced and impart huge savings for a variety of Army applications.

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In-situ OTDR for low-cost optical networks using a single-mode 850-nm VCSEL

Proposed for publication in Electronics Letters.

Keeler, Gordon A.; Serkland, Darwin K.; Geib, K.M.; Peake, Gregory M.

A new approach to optical time-domain reflectometry (OTDR) is proposed that will enable distributed fault monitoring in singlemode VCSEL-based networks. In situ OTDR uses the transmitter VCSEL already resident in data transceivers as both emitter and resonant-cavity photodiode for fault location measurements. Also valuable at longer wavelengths, the concept is demonstrated here using an 850 nm oxide-confined VCSEL and simple electronics. The dead times and sensitivity obtained are adequate to detect the majority of faults anticipated in local- and metropolitan-area networks.

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Development of bottom-emitting 1300-nm vertical-cavity surface-emitting lasers

IEEE Photonics Technology Letters

Louderback, D.A.; Fish, M.A.; Klem, John F.; Serkland, Darwin K.; Choquette, K.D.; Pickrell, G.W.; Stone, R.V.; Guilfoyle, P.S.

We present experimental results on the development of bottom-emitting GaInNAs vertical-cavity surface-emitting lasers (VCSELs) operating at wavelengths near 1300 nm. This development effort is based on the modification of oxide-apertured top-emitting structures to allow emission through the GaAs substrate. Similar device performance was seen in both the top- and bottom-emitting structures. Single-mode output powers (adjusted for substrate absorption) of ∼0.75 mW, with threshold currents of 1.3 mA, were achieved with ∼3.5-μm aperture diameters. Larger multimode devices exhibited a maximum adjusted output power of 2.2 mW. To the best of our knowledge, these are the first bottom-emitting flip-chip compatible 1300-nm VCSELs fabricated with GaInNAs-GaAs active regions.

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Final report on LDRD project 52722 : radiation hardened optoelectronic components for space-based applications

Blansett, Ethan B.; Klem, John F.; Hawkins, Samuel D.; Sanchez, Victoria S.; Sullivan, Charles T.; Wrobel, Theodore F.; Blansett, Ethan B.; Serkland, Darwin K.; Keeler, Gordon A.; Geib, K.M.; Karpen, Gary D.; Diaz, Melissa R.; Peake, Gregory M.; Hargett, Terry H.

This report describes the research accomplishments achieved under the LDRD Project 'Radiation Hardened Optoelectronic Components for Space-Based Applications.' The aim of this LDRD has been to investigate the radiation hardness of vertical-cavity surface-emitting lasers (VCSELs) and photodiodes by looking at both the effects of total dose and of single-event upsets on the electrical and optical characteristics of VCSELs and photodiodes. These investigations were intended to provide guidance for the eventual integration of radiation hardened VCSELs and photodiodes with rad-hard driver and receiver electronics from an external vendor for space applications. During this one-year project, we have fabricated GaAs-based VCSELs and photodiodes, investigated ionization-induced transient effects due to high-energy protons, and measured the degradation of performance from both high-energy protons and neutrons.

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OMVPE of GaAsSbN for long wavelength emission on GaAs

Proposed for publication in the Journal of Crystal Growth.

Peake, Gregory M.; Peake, Gregory M.; Waldrip, Karen E.; Hargett, Terry H.; Modine, N.A.; Serkland, Darwin K.

GaAsSbN was grown by organometallic vapor phase epitaxy (OMVPE) as an alternative material to InGaAsN for long wavelength emission on GaAs substrates. OMVPE of GaAsSbN using trimethylgallium, 100% arsine, trimethylantimony, and 1,1-dimethylhydrazine was found to be kinetically limited at growth temperatures ranging from 520 C to 600 C, with an activation energy of 10.4 kcal/mol. The growth rate was linearly dependent on the group III flow and has a complex dependence on the group V constituents. A room temperature photoluminescence wavelength of >1.3 {micro}m was observed for unannealed GaAs{sub 0.69}Sb{sub 0.3}N{sub 0.01}. Low temperature (4 K) photoluminescence of GaAs{sub 0.69}Sb{sub 0.3}N{sub 0.01} shows an increase in FWHM of 2.4-3.4 times the FWHM of GaAs{sub 0.7}Sb{sub 0.3}, a red shift of 55-77 meV, and a decrease in intensity of one to two orders of magnitude. Hall measurements indicate a behavior similar to that of InGaAsN, a 300 K hole mobility of 350 cm{sup 2}/V-s with a 1.0 x 10{sup 17}/cm{sup 3} background hole concentration, and a 77 K mobility of 1220 cm{sup 2}/V-s with a background hole concentration of 4.8 x 10{sup 16}/cm{sup 3}. The hole mass of GaAs{sub 0.7}Sb{sub 0.3}/GaAs heterostructures was estimated at 0.37-0.40m{sub o}, and we estimate an electron mass of 0.2-0.3m{sub o} for the GaAs{sub 0.69}Sb{sub 0.3}N{sub 0.01}/GaAs system. The reduced exciton mass for GaAsSbN was estimated at about twice that found for GaAsSb by a comparison of diamagnetic shift vs. magnetic field.

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Final Report on LDRD Project: High-Bandwidth Optical Data Interconnects for Satellite Applications

Sanchez, Victoria S.; Sullivan, Charles T.; Allerman, A.A.; Rienstra, Jeffrey L.; Serkland, Darwin K.; Geib, K.M.; Blansett, Ethan B.; Karpen, Gary D.; Peake, Gregory M.; Hargett, Terry H.

This report describes the research accomplishments achieved under the LDRD Project ''High-Bandwidth Optical Data Interconnects for Satellite Applications.'' The goal of this LDRD has been to address the future needs of focal-plane-array (FPA) sensors by exploring the use of high-bandwidth fiber-optic interconnects to transmit FPA signals within a satellite. We have focused primarily on vertical-cavity surface-emitting laser (VCSEL) based transmitters, due to the previously demonstrated immunity of VCSELs to total radiation doses up to 1 Mrad. In addition, VCSELs offer high modulation bandwidth (roughly 10 GHz), low power consumption (roughly 5 mW), and high coupling efficiency (greater than -3dB) to optical fibers. In the first year of this LDRD, we concentrated on the task of transmitting analog signals from a cryogenic FPA to a remote analog-to-digital converter. In the second year, we considered the transmission of digital signals produced by the analog-to-digital converter to a remote computer on the satellite. Specifically, we considered the situation in which the FPA, analog-to-digital converter, and VCSEL-based transmitter were all cooled to cryogenic temperatures. This situation requires VCSELs that operate at cryogenic temperature, dissipate minimal heat, and meet the electrical drive requirements in terms of voltage, current, and bandwidth.

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Effective index model predicts modal frequencies of vertical-cavity lasers

Applied Physics Letters

Serkland, Darwin K.; Hadley, G.R.; Choquette, K.D.; Geib, K.M.; Allerman, A.A.

Previously, an effective index optical model was introduced for the analysis of lateral waveguiding effects in vertical-cavity surface-emitting lasers. The authors show that the resultant transverse equation is almost identical to the one typically obtained in the analysis of dielectric waveguide problems, such as a step-index optical fiber. The solution to the transverse equation yields the lateral dependence of the optical field and, as is recognized in this paper, the discrete frequencies of the microcavity modes. As an example, they apply this technique to the analysis of vertical-cavity lasers that contain thin-oxide apertures. The model intuitively explains the experimental data and makes quantitative predictions in good agreement with a highly accurate numerical model.

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111 Results
111 Results