Publications

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The success of dynamic materials properties research at Sandia National Laboratories has led to research into ultra-low impedance, compact pulsed power systems capable of multi-MA shaped current pulses with rise times ranging from 220-500 ns. The Genesis design consists of two hundred and forty 200 kV, 80 kA modules connected in parallel to a solid dielectric disk transmission line and is capable of producing 280 kbar of magnetic pressure (>500 kbar pressure in high Z materials) in a 1.75 nH, 20 mm wide stripline load. Stripline loads operating under these conditions expand during the experiment resulting in a time-varying load that can impact the performance and lifetime of the system. This paper provides analysis of time-varying stripline loads and the impact of these loads on system performance. Further, an approach to reduce dielectric stress levels through active damping is presented as a means to increase system reliability and lifetime. © 2011 IEEE.

Genesis is a compact pulsed power platform designed by Sandia National Laboratories to generate precision shaped multi-MA current waves with a rise time of 200-500 ns. In this system, two hundred and forty, 200 kV, 80 kA modules are selectively triggered to produce 280 kbar of magnetic pressure (>500 kbar pressure in high Z materials) in a stripline load for dynamic materials properties research. This new capability incorporates the use of solid dielectrics to reduce system inductance and size, programmable current shaping, and gas switches that must perform over a large range of operating conditions. Research has continued on this technology base with a focus on demonstrating the integrated performance of key concepts into a Genesis-like prototype called Protogen. Protogen measures approximately 1.4 m by 1.4 m and is designed to hold twelve Genesis modules. A fixed inductance load will allow rep-rate operation for component reliability and system lifetime experiments at the extreme electric field operating conditions expected in Genesis. © 2011 IEEE.

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The Hugoniot response of materials is centrally important in the field of high pressure science. Highly accurate Hugoniot measurements not only provide better material references but also allow for the detection of subtle material phenomena. A process has been developed utilizing the Sandia Z accelerator to measure Hugoniot response at multi-megabar pressure resulting in extremely high accuracy data. Key considerations are the use of large surface area flyer plates allowing measurement configurations with multiple targets and diagnostics. This allows for greatly reduced uncertainty in the data. The details of this process are given and each aspect is closely examined focusing on the individual contributions to the overall accuracy of the result. © 2010 IOP Publishing Ltd.

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In order to generate new properties of metals exposed to high pressure states, it is desirable to study samples loaded in one-dimensional strain. Previous work to obtain these ideal conditions, involve a technique where the sample was recovered at late times to examine its microstructure. In those experiments, the shock-loading was produced by impacting the sample with a flyer plate. In the present work, we modified the sample recovery assembly and optimized it for ramp wave loading. We describe the 2-D calculations performed with the ALEGRA MHD code that led to improved recovery assembly efficiency. Preliminary comparisons of the simulations with measurements of the sample deformation from an experiment indicate excellent agreement. © 2009 American Institute of Physics.

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The Z Refurbishment Project was completed in September 2007. Prior to the shutdown of the Z facility in July 2006 to install the new hardware, it provided currents of {le} 20 MA to produce energetic, intense X-ray sources ({approx} 1.6 MJ, > 200 TW) for performing high energy density science experiments and to produce high magnetic fields and pressures for performing dynamic material property experiments. The refurbishment project doubled the stored energy within the existing tank structure and replaced older components with modern, conventional technology and systems that were designed to drive both short-pulse Z-pinch implosions and long-pulse dynamic material property experiments. The project goals were to increase the delivered current for additional performance capability, improve overall precision and pulse shape flexibility for better reproducibility and data quality, and provide the capacity to perform more shots. Experiments over the past year have been devoted to bringing the facility up to full operating capabilities and implementing a refurbished suite of diagnostics. In addition, we have enhanced our X-ray backlighting diagnostics through the addition of a two-frame capability to the Z-Beamlet system and the addition of a high power laser (Z-Petawatt). In this paper, we will summarize the changes made to the Z facility, highlight the new capabilities, and discuss the results of some of the early experiments.

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Veloce is a medium-voltage, high-current, compact pulsed power generator developed for isentropic and shock compression experiments. Because of its increased availability and ease of operation, Veloce is well suited for studying isentropic compression experiments (ICE) in much greater detail than previously allowed with larger pulsed power machines such as the Z accelerator. Since the compact pulsed power technology used for dynamic material experiments has not been previously used, it is necessary to examine several key issues to ensure that accurate results are obtained. In the present experiments, issues such as panel and sample preparation, uniformity of loading, and edge effects were extensively examined. In addition, magnetohydrodynamic (MHD) simulations using the ALEGRA code were performed to interpret the experimental results and to design improved sample/panel configurations. Examples of recent ICE studies on aluminum are presented.

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Complementary gas-gun and electro-magnetic pulse tests conducted in Sandia's Dynamic Integrated Compression Experimental (DICE) Facility have, respectively, probed the behavior of electronic-grade Kovar samples under controlled impact and intermediate-strain-rate ICE (Isentropic Compression Experiment) loading. In all tests, velocity interferometer (VISAR) diagnostics provided time-resolved measurements of sample response for conditions involving one-dimensional (i:e:, uniaxial strain) compression and release. Wave-profile data from the gas-gun impact experiments have been analyzed to assess the Hugoniot Elastic Limit (HEL), Hugoniot equation of state, spall strength, and high-pressure yield strength of shocked Kovar. The ICE wave-profile data have been interpreted to determine the locus of isentropic stress-strain states generated in Kovar for deformation rates substantially lower than those associated with a shock process. The impact and ICE results have been compared to examine the influence of loading rate on high-pressure strength.

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Binders such as Estane, Teflon, Kel F and HTPB are typically used in heterogeneous explosives to bond polycrystalline constituents together as an energetic composite. Combined theoretical and experimental studies are underway to unravel the mechanical response of these materials when subjected to isentropic compression loading. Key to this effort is the determination of appropriate constitutive and EOS property data at extremely high stress-strain states as required for detailed mesoscale modeling. The Sandia Z accelerator and associated diagnostics provides new insights into mechanical response of these nonreactive constituents via isentropic ramp-wave compression loading. Several thicknesses of samples, varied from 0.3 to 1.2 mm, were subjected to a ramp load of {approx}42 Kbar over 500 ns duration using the Sandia Z-machine. Profiles of transmitted ramp waves were measured at window interfaces using conventional VISAR. Shock physics analysis is then used to determine the nonlinear material response of the binder materials. In this presentation we discuss experimental and modeling details of the ramp wave loading ICE experiments designed specifically for binder materials.

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The shock compaction behavior of a tungsten carbide powder was investigated using a new experimental design for gas-gun experiments. This design allows the Hugoniot properties to be measured with reasonably good accuracy despite the inherent difficulties involved with distended powders. The experiments also provide the first reshock state for the compacted powder. Experiments were conducted at impact velocities of 245, 500, and 711 m/s. A steady shock wave was observed for some of the sample thicknesses, but the remainder were attenuated due to release from the back of the impactor or the edge of the sample. The shock velocity for the powder was found to be quite low, and the propagating shock waves were seen to be very dispersive. The Hugoniot density for the 711 m/s experiment was close to ambient crystal density for tungsten carbide, indicating nearly complete compaction. When compared with quasi-static compaction results for the same material, the dynamic compaction data is seen to be significantly stiffer for the regime over which they overlap. Based on these initial results, recommendations are made for improving the experimental technique and for future work to improve our understanding of powder compaction.

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Of special promise for providing dynamic mesoscale response data is the line-imaging VISAR, an instrument for providing spatially resolved velocity histories in dynamic experiments. We have prepared two line-imaging VISAR systems capable of spatial resolution in the 10-20 micron range, at the Z and STAR facilities. We have applied this instrument to selected experiments on a compressed gas gun, chosen to provide initial data for several problems of interest, including: (1) pore-collapse in copper (two variations: 70 micron diameter hole in single-crystal copper) and (2) response of a welded joint in dissimilar materials (Ta, Nb) to ramp loading relative to that of a compression joint. The instrument is capable of resolving details such as the volume and collapse history of a collapsing isolated pore.

The high-pressure response of cryogenic liquid deuterium (LD{sub 2}) has been studied to pressures of {approx}400GPa and densities of {approx}1.5g/cm{sup 3}. Using intense magnetic pressure produced by the Sandia National Laboratories Z accelerator, macroscopic aluminum or titanium flyer plates, several mm in lateral dimensions and a few hundred microns in thickness, have been launched to velocities in excess of 22 km/s, producing constant pressure drive times of approximately 30 ns in plate impact, shock wave experiments. This flyer plate technique was used to perform shock wave experiments on LD{sub 2} to examine its high-pressure equation of state. Using an impedance matching method, Hugoniot measurements of LD{sub 2} were obtained in the pressure range of {approx}22-100GPa. Results of these experiments indicate a peak compression ratio of approximately 4.3 on the Hugoniot. In contrast, previously reported Hugoniot states inferred from laser-driven experiments indicate a peak compression ratio of approximately 5.5-6 in this same pressure range. The stiff Hugoniot response observed in the present impedance matching experiments was confirmed in simultaneous, independent measurements of the relative transit times of shock waves reverberating within the sample cell, between the front aluminum drive plate and the rear sapphire window. The relative timing was found to be sensitive to the density compression along the principal Hugoniot. Finally, mechanical reshock measurements of LD{sub 2} using sapphire, aluminum, and {alpha}-quartz anvils were made. These results also indicate a stiff response, in agreement with the Hugoniot and reverberating wave measurements. Using simple model-independent arguments based on wave propagation, the principal Hugoniot, reverberating wave, and sapphire anvil reshock measurements are shown to be internally self-consistent, making a strong case for a Hugoniot response with a maximum compression ratio of {approx}4.3-4.5. The trends observed in the present data are in very good agreement with several ab initio models and a recent chemical picture model for LD{sub 2}, but in disagreement with previously reported laser-driven shock results. Due to this disagreement, significant emphasis is placed on the discussion of uncertainties, and the potential systematic errors associated with each measurement.

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The pulsed-power Z machine, in an isentropic compression experiment (ICE) mode, will allow the dynamic characterization of porous materials - here various ceramic powders, e.g., Al{sub 2}O{sub 3}, WC, ZrO{sub 2} - at roughly half their solid densities. A cylindrical configuration can provide megabar-level loads on an annulus of the sample material. Data will be provided by velocity interferometers that measure free-surface (or possibly interface) particle velocities. Differing sample thicknesses using stepped or conical geometries yield experimental efficiency by allowing multiple data records on single shots. With the p/{alpha} model for porous materials, the one-dimensional Lagrangian hydrocode WONDY provides the needed analyses. Based on static data, both power-law and quadratic crush curves are employed. Within the model constraints, we suggest that the most important parameter for characterizing the material is the crush strength, p{sub s}. With adequate sample thicknesses, the planned velocity measurements differentiate among the various assumptions for p{sub s}.

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Using intense magnetic pressure, a method was developed to launch flyer plates to velocities in excess of 20 km s{sup -1}. This technique was used to perform plate-impact, shock wave experiments on cryogenic liquid deuterium (LD{sub 2}) to examine its high-pressure equation of state (EOS). Using an impedance matching method, Hugoniot measurements were obtained in the pressure range of 22--100 GPa. The results of these experiments disagree with the previously reported Hugoniot measurements of LD2 in the pressure range above {approx}40 GPa, but are in good agreement with first principles, ab initio models for hydrogen and its isotopes.

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Two experiments have been performed to measure the effects of pulsed radiation loads on the front of small tubular structures, using as an energy source the X-ray fluence produced by a Z-pinch at the Sandia National Laboratories Z Facility. The project had two major goals: to establish the feasibility of using the Z machine to study the phenomenology associated with debris generation and propagation down tubular structures with partitions; and to use the resultant experimental data to validate numerical hydrocodes (shock physics codes) so that we have confidence in their use in analyzing these types of situations. Two tubular aluminum structures (5 and 10 cm long and 1 cm inside diameter) were prepared, with aluminum partitions located at the front, halfway down the pipe, and at the rear. Interferometry (VISARs) provided multiple velocity histories for all of the partitions. In both experiments, the first barrier, which was exposed directly to the x-ray fluence, was launched into the pipe at a velocity of ∼2 km/s, accelerating to give a mean velocity of ∼ 2.6 km/s. Loss of plate integrity is inferred from the dispersed launch of the second partition at ∼1 km/s. Wall shocks propagating at 4.5 km/s were inferred. Post-test metallography showed evidence of melting and partial vaporization of the plates, and turbulent mixing with material from the walls. Calculations qualitatively agree with the observed results, but slightly overpredict debris velocity, possibly due to overestimates of total energy fluence. An application for this work is the study of techniques for line-of-sight shock and debris mitigation on high-power pulsed power facilities such as Z and its follow-on machines. © 2001 Elsevier Science Ltd. All rights reserved.

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A long-standing goal of the equation of state (EOS) community has been the development of a loading capability for direct measurement of material properties along an isentrope. Previous efforts on smooth bore launchers have been somewhat successful, but quite difficult to accurately reproduce, had pressure limitations, or tended to be a series of small shocks as opposed to a smoothly increasing pressure load. A technique has recently been developed on the Sandia National Laboratories Z accelerator which makes use of the high current densities and magnetic fields available to produce nearly isentropic compression of samples that are approximately 1 mm in thickness over approximately 120 ns. Velocity interferometry is used to measure the rear surface motion of these samples. The resulting time resolved velocity profiles from multiple sample thicknesses provide information about mechanical response under isentropic loading conditions and phase transition kinetics. Feasibility experiments have been performed to pressures of approximately 130 kbar in copper and 300 kbar in iron with effects of the {alpha}-{var_epsilon} phase change kinetics in iron clearly observed. Work is in progress to achieve 1--2% accuracy in P-v space along an isentrope, provide uniaxial strain, and to eliminate magnetic field and current diffusion within the sample of interest.