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Soft elasticity optimises dissipation in 3D-printed liquid crystal elastomers

Nature Communications

Mistry, D.; Traugutt, N.A.; Sanborn, Brett S.; Volpe, R.H.; Chatham, L.S.; Zhou, R.; Song, Bo S.; Yu, K.; Long, K.N.; Yakacki, C.M.

Soft-elasticity in monodomain liquid crystal elastomers (LCEs) is promising for impact-absorbing applications where strain energy is ideally absorbed at constant stress. Conventionally, compressive and impact studies on LCEs have not been performed given the notorious difficulty synthesizing sufficiently large monodomain devices. Here, we use direct-ink writing 3D printing to fabricate bulk (>cm3) monodomain LCE devices and study their compressive soft-elasticity over 8 decades of strain rate. At quasi-static rates, the monodomain soft-elastic LCE dissipated 45% of strain energy while comparator materials dissipated less than 20%. At strain rates up to 3000 s−1, our soft-elastic monodomain LCE consistently performed closest to an ideal-impact absorber. Drop testing reveals soft-elasticity as a likely mechanism for effectively reducing the severity of impacts – with soft elastic LCEs offering a Gadd Severity Index 40% lower than a comparable isotropic elastomer. Lastly, we demonstrate tailoring deformation and buckling behavior in monodomain LCEs via the printed director orientation.

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Dynamic high-rate tensile characterization of metallic materials with a Kolsky tension bar

Advances in Experimental Impact Mechanics

Song, Bo S.

Kolsky bar techniques have been developed and utilized for characterizing the dynamic behavior of materials at high strain rates, primarily in compression. Recently dynamic tensile technique with Kolsky tension bars has been significantly advanced, particularly for metallic materials. Dynamic tensile characterization of metallic materials provides not only high-strain-rate stress-strain property but also failure/fracture response. In this chapter, the most recent advance in Kolsky tension bar techniques is presented, including Kolsky tension bar design, specimen design, and mounting methods, and challenges in dynamic tensile tests and data reduction process, for cylindrical and flat specimens, respectively. Interrupted Kolsky tension bar techniques are also presented for investigating strain-rate-dependent damage evolution, structure-property relationship, as well as multiscale failure and fracture.

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Mechanical characterization of 304L-VAR stainless steel in tension with a full coverage of low, intermediate, and high strain rates

Mechanics of Materials

Jin, H.; Sanborn, Brett S.; Lu, W.Y.; Song, Bo S.

A 304L-VAR stainless steel is mechanically characterized in tension over a full range of strain rates from low, intermediate, to high using a variety of apparatuses. While low- and high-strain-rate tests are conducted with a conventional Instron and a Kolsky tension bar, the tensile tests at intermediate strain rates are conducted with a fast MTS and a Drop-Hopkinson bar. The fast MTS used in this study is able to obtain reliable tensile response at the strain rates up to 150 s−1, whereas the lower limit for the Drop-Hopkinson bar is 100 s−1. Combining the fast MTS and the Drop-Hopkinson bar closes the gap within the intermediate strain rate regime. Using these four apparatuses, the tensile stress-strain curves of the 304L-VAR stainless steel are obtained at strain rates on each order of magnitude ranging from 0.0001 to 2580 s−1. All tensile stress-strain curves exhibit linear elasticity followed by significant work hardening prior to necking. After necking occurrs, the specimen load decreases, and the deformation becomes highly localized until fracture. The tensile stress-strain response of the 304L-VAR stainless steel exhibits strain rate dependence. The flow stress increases with increasing strain rate and is described with a power law. The strain-rate sensitivity is also strain-dependent, possibly due to thermosoftening caused by adiabatic heating at high strain rates. The 304L-VAR stainless steel shows significant ductility. The true strains at the onset of necking and at failure are determined. The results show that the true strains at both onset of necking and failure decrease with increasing strain rate. The true failure strains are approximately 200% at low strain rates but are significantly lower (~100%) at high strain rates. The transition of true failure strain occurs within the intermediate strain rate range between 10−2 and 102 s−1. A Boltzmann description is used to present the effect of nominal strain rate on true failure strain.

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Dynamic Tensile Characterization of Thin-Sheet Brittle Metallic Materials

Experimental Techniques

Sanborn, Brett S.; Hudspeth, M.; Song, Bo S.

Refractory metals are favorable materials in applications where high strength and ductility are needed at elevated temperatures. In some cases, operating temperatures may be near the melting point of the material. However, as temperature drops, refractory metals typically undergo a significant mechanical response change - ductile-to-brittle transition. These materials may be subjected to high strain rate loading at an ambient temperature state, such as an impact or crash. Knowledge of the high rate material properties are essential for design as well as simulation of impact events. The high rate stress-strain behavior of brittle metallic materials at ambient temperature is rarely studied because of experimental challenges, particularly when failure is involved. Failure typically occurs within the non-gage section of the material, which invalidates any collected stress-strain information. In this study, a method to determine a specimen geometry which will produce failures in the gage section is presented. Pure tungsten in thin-sheet form was used as a trial material to select a specimen geometry for high rate Kolsky tension bar experiments. A finite element simulation was conducted to derive a strain correction for more accurate results. The room temperature stress-strain behavior of pure tungsten at a strain rate of 24 s−1 is presented. The outcome of this experimental technique can be applied to other brittle materials for dynamic tensile characterization.

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A Novel Design of Guiding Stress Wave Propagation

Journal of Dynamic Behavior of Materials

Li, Y.; Ngo, E.; Song, Bo S.

Impact loads can induce a series of undesirable physical phenomena including vibration, acoustical shock, perforation, fracture and fragmentation, etc. The energy associated with the impact loads can lead to severe structure damage and human injuries. A design approach which effectively reduces these negative impacts through shock/stress wave diversion is highly needed. In this paper, a computational model which predicts stress wave propagation by considering different beam geometries and configurations is developed. A novel concept of wave guide design which modifies the stress wave propagation path without disturbance is also presented. This design approach is not only useful for material property characterization particularly at intermediate or high strain rates, but also allows stress wave propagation in a desired direction as the shock/impact energy can be redistributed in controllable paths. The numerical results are experimentally verified through a Drop-Hopkinson bar apparatus at Sandia National Laboratories.

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Dynamic Tensile Response of a Fe–49Co–2V Alloy at Various Strain Rates and Temperatures

Journal of Dynamic Behavior of Materials

Song, Bo S.; Sanborn, Brett S.; Susan, D.F.; Johnson, Kyle J.; Dabling, Jeffrey D.; Carroll, Jay D.; Brink, Adam R.; Grutzik, S.; Kustas, Andrew K.

Soft ferromagnetic alloys are often utilized in electromagnetic applications due to their desirable magnetic properties. In support of these applications, the ferromagnetic alloys are also required to bear mechanical load under various loading and environmental conditions. In this study, a Fe–49Co–2V alloy was dynamically characterized in tension with a Kolsky tension bar and a Drop–Hopkinson bar at various strain rates and temperatures. Dynamic tensile stress–strain curves of the Fe–49Co–2V alloy were obtained at strain rates ranging from 40 to 230 s−1 and temperatures from − 100 to 100 °C. All dynamic tensile stress–strain curves exhibited an initial linear elastic response to an upper yield followed by Lüders band response and then a nearly linear work-hardening behavior. The yield strength of this material was found to be sensitive to both strain rate and temperature, whereas the hardening rate was independent of strain rate or temperature. The Fe–49Co–2V alloy exhibited a feature of brittle fracture in tension under dynamic loading with no necking being observed.

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Dynamic Tensile Behavior of Soft Ferromagnetic Alloy Fe-Co-2V

Conference Proceedings of the Society for Experimental Mechanics Series

Sanborn, Brett S.; Song, Bo S.; Susan, D.F.; Johnson, Kyle J.; Dabling, Jeffrey D.; Carroll, Jay D.; Brink, Adam R.; Grutzik, Scott J.; Kustas, Andrew K.

Fe-Co-2V is a soft ferromagnetic alloy used in electromagnetic applications due to excellent magnetic properties. However, the discontinuous yielding (Luders bands), grain-size-dependent properties (Hall-Petch behavior), and the degree of order/disorder in the Fe-Co-2V alloy makes it difficult to predict the mechanical performance, particularly in abnormal environments such as elevated strain rates and high/low temperatures. Thus, experimental characterization of the high strain rate properties of the Fe-Co-2V alloy is desired, which are used for material model development in numerical simulations. In this study, the high rate tensile response of Fe-Co-2V is investigated with a pulse-shaped Kolsky tension bar over a wide range of strain rates and temperatures. Effects of temperature and strain rate on yield stress, ultimate stress, and ductility are discussed.

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Correction of specimen strain measurement in Kolsky tension bar experiments on work-hardening materials

International Journal of Impact Engineering

Song, Bo S.; Sanborn, Brett S.; Susan, D.F.; Johnson, Kyle J.; Dabling, Jeffrey D.; Carroll, Jay D.; Brink, Adam R.; Grutzik, Scott J.; Kustas, Andrew K.

Cylindrical dog-bone (or dumbbell) shaped samples have become a common design for dynamic tensile tests of ductile materials with a Kolsky tension bar. When a direct measurement of displacement between the bar ends is used to calculate the specimen strain, the actual strain in the specimen gage section is overestimated due to strain in the specimen shoulder and needs to be corrected. The currently available correction method works well for elastic-perfectly plastic materials but may not be applicable to materials that exhibit significant work-hardening behavior. In this study, we developed a new specimen strain correction method for materials possessing an elastic-plastic with linear work-hardening stress–strain response. A Kolsky tension bar test of a Fe-49Co-2V alloy (known by trade names Hiperco and Permendur) was used to demonstrate the new specimen strain correction method. This new correction method was also used to correct specimen strains in Kolsky tension bar experiments on two other materials: 4140 alloy, and 304L-VAR stainless steel, which had different work-hardening behavior.

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A Modified Johnson–Cook Model for Dynamic Response of Metals with an Explicit Strain- and Strain-Rate-Dependent Adiabatic Thermosoftening Effect

Journal of Dynamic Behavior of Materials

Song, Bo S.; Sanborn, Brett S.

Metallic alloys are extensively utilized in applications where extreme loading and environmental conditions occur and engineering reliability of components or structures made of such materials is a significant concern in applications. Adiabatic heating in these materials during high-rate deformation is of great interest to analysts, experimentalists, and modelers due to a reduction in strength that is produced. Capturing the thermosoftening caused by adiabatic heating is critical in material model development to precisely predict the dynamic response of materials and structures at high rates of loading. In addition to strain rate effect, the Johnson–Cook (JC) model includes a term to describe the effect of either environmental or adiabatic temperature rise. The standard expression of the JC model requires quantitative knowledge of temperature rise, but it can be challenging to obtain in situ temperature measurements, especially in dynamic experiments. The temperature rise can be calculated from plastic work with a predetermined Taylor-Quinney (TQ) coefficient. However, the TQ coefficient is difficult to determine since it may be strain and strain-rate dependent. In this study, we modified the JC model with a power-law strain rate effect and an explicit form of strain- and strain-rate-dependent thermosoftening due to adiabatic temperature rise to describe the strain-rate-dependent tensile stress–strain response, prior to the onset of necking, for 304L stainless steel, A572, and 4140 steels. The modified JC model was also used to describe the true stress–strain response during necking for A572 and 4140 steels at various strain rates. The results predicted with the modified JC model agreed with the tensile experimental data reasonably well.

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Experimental Measurement and Analysis of Stress/Shock Wave Propagation Speed through Pre-strained Silicone Foam Pads under Lateral Confinement

Journal of Dynamic Behavior of Materials

Song, Bo S.; Sanborn, Brett S.; Lu, Wei-Yang L.

Foam materials are extensively utilized in aerospace, military, and transportation applications to mitigate blast or shock impact. When foam materials are subjected to an external high-speed impact, shock, or blast loading, an elastic wave or shock wave will form and propagate through the thickness of the foam materials. In this study, silicone foam pads, which were confined laterally and pre-strained to different levels, were experimentally characterized and theoretically analyzed to understand their effects on wave propagation characteristics under impact loading. Depending on impact velocity, either an elastic strain wave or a shock wave would be generated in the silicone foam pad with different pre-strains. Above a certain impact velocity, a shock wave will be generated whereas, below this threshold impact velocity, an elastic strain wave will be generated. This threshold impact velocity depends on the pre-strain applied to the silicone foam pad. Equations are provided to estimate the wave propagation speed for either an elastic or a shock wave from the amount of pre-strain in the silicone foam pads and the impact velocity. These equations are expected to help improve silicone foam design and assembly processes for shock or blast mitigation applications.

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Energy Dissipation Characteristics in Pre-strained Silicone Foam Transitioning to Silicone Rubber

Journal of Dynamic Behavior of Materials

Sanborn, Brett S.; Song, Bo S.

Silicone foam is used as a shock mitigation material in a variety of systems to protect internal components from being damaged during external shock or impact loading. Characterizing the shock mitigation response of silicone foam under a variety of scenarios is a critical step in designing and/or evaluating new shock mitigation systems. In this study, a Kolsky bar with pre-compression capability was used with a passive radial confinement tube to subject the sample to various levels of pre-strain followed by impact loading. The effects of both pre-strain and impact velocity on impact energy dissipation behavior were investigated for silicone foam. The energy dissipation response of silicone foam is compared to a silicone rubber manufactured using the same processing methods to understand the energy dissipation characteristics of silicone foams transitioning to a silicone rubber. The final density of the foam or rubber plays a key role in both the total energy dissipation ratio in the time domain and the energy dissipation ratio as a function of frequency in the frequency domain.

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Dynamic Tensile Characterization of Hiperco 50A Alloy at Various Strain Rates and Temperatures

Song, Bo S.; Sanborn, Brett S.

Soft ferromagnetic alloys are often utilized in electromagnetic applications due to their desirable magnetic properties. In support of these applications, the ferromagnetic alloys are also desired to bear mechanical load at various environmental temperatures. In this study, a Permendur 2V alloy manufactured by Metalwerks Inc. (but referred to Hiperco 50A, a trademark of Carpenter Technologies Inc.) was dynamically characterized in tension with a Kolsky tension bar and a Dropkinson bar at various strain rates and temperatures. Dynamic tensile stress-strain curves of the Hiperco 50A alloy were obtained at the strain rates ranging from 40 to 230 s -1 and temperatures from -100 to 100degC. All tensile stress-strain curves exhibited an initial linear elastic response to an upper yield followed by a Eiders banding response and then a nearly linear work-hardening behavior. The yield strength of this material was found to be sensitive to both strain rate and temperature; whereas, the hardening rate was independent of strain rate or temperature. The Hiperco 50A alloy exhibited a feature of brittle fracture in tension under dynamic loading with no necking being observed. ACKNOWLEDGEMENTS The authors acknowledge Kyle Johnson, Jefferey Dab ling, Donald Susan, Jay Carroll, Adam Brink, Scott Grutzik, and Andrew Kustas for the valuable discussion of test plan and results. Thanks Donald Susan for specimen preparation for this project. The authors also thanks Randy Everett for his support to the operation of dynamic tests in this proj ect.

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Radial Inertia Effect on Dynamic Compressive Response of Polymeric Foam Materials

Experimental Mechanics

Song, Bo S.; Sanborn, Brett S.; Lu, Wei-Yang L.

Polymeric foams have been extensively used in shock isolation applications because of their superior shock or impact energy absorption capability. However, as a type of soft condensed matter, the highly nonlinear, heterogeneous, and dissipative behavior of polymeric foams may result in an ineffective mitigation or isolation to shock/blast loading. To meet certain desired shock mitigation or isolation requirements, the polymeric foams need to be experimentally characterized to obtain their intrinsic material response. However, radial inertia during dynamic compression has become a severe issue and needs to be fully understood. In this study, we developed an analytical method to calculate the additional stress induced by radial inertia in a polymeric foam specimen. The radial inertia is generally caused by Poisson’s effect and associated with three different mechanisms – axial strain acceleration, large deformation, and Poisson’s ratio change. The effect of Poisson’s ratio change during deformation on radial inertia was specifically investigated for hyperelastic foam materials, and verified with experimental results obtained from Kolsky compression bar tests on a silicone foam.

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Quasi-static and dynamic poisson’s ratio evolution of hyperelastic foams

Conference Proceedings of the Society for Experimental Mechanics Series

Sanborn, Brett S.; Song, Bo S.

Poisson’s ratio of soft, hyperelastic foam materials such as silicone foam is typically assumed to be both a constant and a small number near zero. However, when the silicone foam is subjected to large deformation into densification, the Poisson’s ratio may significantly change, which warrants careful and appropriate consideration in modeling and simulation of impact/shock mitigation scenarios. The evolution of the Poisson’s ratio of foam materials has not yet been characterized. In this study, radial and axial measurements of specimen strain are made simultaneously during quasi-static and dynamic compression test on a silicone foam. The Poisson’s ratio was found to exhibit a transition from compressible to nearly incompressible based on strain level and reached different values at quasi-static and dynamic rates.

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Poisson's ratio of a hyperelastic foam under quasi-static and dynamic loading

International Journal of Impact Engineering

Sanborn, Brett S.; Song, Bo S.

Poisson's ratio is a material constant representing compressibility of material volume. However, when soft, hyperelastic materials such as silicone foam are subjected to large deformation into densification, the Poisson's ratio may rather significantly change, which warrants careful consideration in modeling and simulation of impact/shock mitigation scenarios where foams are used as isolators. The evolution of Poisson's ratio of silicone foam materials has not yet been characterized, particularly under dynamic loading. In this study, radial and axial measurements of specimen strain are conducted simultaneously during quasi-static and dynamic compression tests to determine the Poisson's ratio of silicone foam. The Poisson's ratio of silicone foam exhibited a transition from compressible to nearly incompressible at a threshold strain that coincided with the onset of densification in the material. Poisson's ratio as a function of engineering strain was different at quasi-static and dynamic rates. The Poisson's ratio behavior is presented and can be used to improve constitutive modeling of silicone foams subjected to a broad range of mechanical loading.

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Revisit of dynamic Brazilian tests of geomaterials

Conference Proceedings of the Society for Experimental Mechanics Series

Sanborn, Brett S.; Jones, Elizabeth M.; Hudspeth, Matthew; Song, Bo S.; Broome, Scott T.

Understanding the dynamic behavior of geomaterials is critical for refining modeling and simulation of applications that involve impacts or explosions. Obtaining material properties of geomaterials is challenging, particularly in tension, due to the brittle and low-strength nature of such materials. Dynamic split tension technique (also called dynamic Brazilian test) has been employed in recent decades to determine the dynamic tensile strength of geomaterials. This is primarily because the split tension method is relatively straightforward to implement in a Kolsky compression bar. Typically, investigators use the peak load reached by the specimen to calculate the tensile strength of the specimen material, which is valid when the specimen is compressed at quasi-static strain rate. However, the same assumption cannot be safely made at dynamic strain rates due to wave propagation effects. In this study, the dynamic split tension (or Brazilian) test technique is revisited. High-speed cameras and digital image correlation (DIC) were used to image the failure of the Brazilian-disk specimen to discover when the first crack occurred relative to the measured peak load during the experiment. Differences of first crack location and time on either side of the sample were compared. The strain rate when the first crack is initiated was also compared to the traditional estimation method of strain rate using the specimen stress history.

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Relationship of compressive stress-strain response of engineering materials obtained at constant engineering and true strain rates

International Journal of Impact Engineering

Song, Bo S.; Sanborn, Brett S.

In this study, a Johnson–Cook model was used as an example to analyze the relationship of compressive stress-strain response of engineering materials experimentally obtained at constant engineering and true strain rates. There was a minimal deviation between the stress-strain curves obtained at the same constant engineering and true strain rates. The stress-strain curves obtained at either constant engineering or true strain rates could be converted from one to the other, which both represented the intrinsic material response. There is no need to specify the testing requirement of constant engineering or true strain rates for material property characterization, provided that either constant engineering or constant true strain rate is attained during the experiment.

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Improved experimental and diagnostic techniques for dynamic tensile stress-strain measurement with a Kolsky tension bar

Measurement Science and Technology

Qiu, Ying; Loeffler, Colin M.; Nie, Xu; Song, Bo S.

Kolsky tension bar experiments were improved for dynamic tensile stress-strain measurements with higher fidelity and minimal uncertainties. The difficulties associated with specimen gripping, relatively short gage section, and geometric discontinuity at the bar ends all compromise the accuracy of the traditional strain measurement method in a Kolsky tension bar experiment. In this study, an improved three-channel splitting-beam laser extensometer technique was developed to directly and independently track the displacement of the incident and transmission bar interfaces. By adopting a dual-channel configuration on the incident bar side, the resolution and measurement range of this laser extensometer were coordinated between the two channels to provide highly precise measurement at both small and large strains under high strain-rate loading condition. On the transmission bar side an amplified channel, similar to that used on the incident bar side, was adopted to measure the transmission bar displacement with high resolution. With this novel design, a maximum resolution of approximately 500 nm can be obtained for the bar displacement measurement, which corresponds to a strain of 0.0079% for a specimen with 6.35 mm gage length. To further improve the accuracy, a pair of lock nuts were used to tighten the tensile specimen to the bars in an effort not only to prevent the specimen from potential pre-torsional deformation and damage during installation, but also to provide better thread engagement between the specimen and the bar ends. As a demonstration of this technique, dynamic tensile stress-strain response of a 304L stainless steel was characterized with high resolution in both elastic and plastic deformations.

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Dynamic Tensile Experimental Techniques for Geomaterials: A Comprehensive Review

Journal of Dynamic Behavior of Materials

Heard, W.; Song, Bo S.; Williams, B.; Martin, B.; Sparks, P.; Nie, X.

This review article is dedicated to the Dynamic Behavior of Materials Technical Division for celebrating the 75th anniversary of the Society for Experimental Mechanics (SEM). Understanding dynamic behavior of geomaterials is critical for analyzing and solving engineering problems of various applications related to underground explosions, seismic, airblast, and penetration events. Determining the dynamic tensile response of geomaterials has been a great challenge in experiments due to the nature of relatively low tensile strength and high brittleness. Various experimental approaches have been made in the past century, especially in the most recent half century, to understand the dynamic behavior of geomaterials in tension. In this review paper, we summarized the dynamic tensile experimental techniques for geomaterials that have been developed. The major dynamic tensile experimental techniques include dynamic direct tension, dynamic split tension, and spall tension. All three of the experimental techniques are based on Hopkinson or split Hopkinson (also known as Kolsky) bar techniques and principles. Uniqueness and limitations for each experimental technique are also discussed.

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Development of a New Method to Investigate the Dynamic Friction Behavior of Interfaces Using a Kolsky Tension Bar

Experimental Mechanics

Sanborn, Brett S.; Song, Bo S.; Nishida, E.E.

To understand interfacial interaction of a bi-material during an impact loading event, the dynamic friction coefficient is one of the key parameters that must be characterized and quantified. In this study, a new experimental method to determine the dynamic friction coefficient between two metals was developed by using a Kolsky tension bar and a custom-designed friction fixture. Polyvinylidene fluoride (PVDF) force sensors were used to measure the normal force applied to the friction tribo pairs and the friction force was measured with conventional Kolsky tension bar method. To evaluate the technique, the dynamic friction coefficient between 4340 steel and 7075-T6 aluminum was investigated at an impact speed of approximately 8 m/s. In addition, the dynamic friction coefficient of the tribo pairs with varied surface roughness was also investigated. The data suggest that higher surface roughness leads to higher friction coefficients at the same speed of 8 m/s.

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Effect of pre-strain, processing conditions, and impact velocity on energy dissipation in silicone foams and rubber

Conference Proceedings of the Society for Experimental Mechanics Series

Sanborn, Brett S.; Song, Bo S.

Silicone foams and rubber are used in a variety of applications to protect internal components from external shock impact. Understanding how these materials mitigate impact energy is a crucial step in designing more effective shock isolation systems for components. In this study, a Kolsky bar with pre-compression and passive radial confinement capabilities was used to investigate the response of silicone foams and rubber subjected to impact loading at different speeds. Using the preload capability, silicone foam samples were subjected to increasing levels of pre-strain. Frequency-based analyses were carried out on results from silicone foams and rubber to study the effect of both pre-strain and material processing conditions on the mechanism of energy dissipation in the frequency domain. Additionally, effects of impact speed on energy dissipation through silicone foams and rubber were investigated.

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Comparative shock response of additively manufactured versus conventionally wrought 304L stainless steel

AIP Conference Proceedings

Wise, Jack L.; Adams, David P.; Nishida, E.E.; Song, Bo S.; Maguire, M.C.; Carroll, Jay D.; Reedlunn, Benjamin R.; Bishop, Joseph E.; Palmer, T.A.

Gas-gun experiments have probed the compression and release behavior of impact-loaded 304L stainless steel specimens that were machined from additively manufactured (AM) blocks as well as baseline ingot-derived bar stock. The AM technology permits direct fabrication of net-or near-net-shape metal parts. For the present investigation, velocity interferometer (VISAR) diagnostics provided time-resolved measurements of sample response for onedimensional (i.e., uniaxial strain) shock compression to peak stresses ranging from 0.2 to 7.0 GPa. The acquired waveprofile data have been analyzed to determine the comparative Hugoniot Elastic Limit (HEL), Hugoniot equation of state, spall strength, and high-pressure yield strength of the AM and conventional materials. The possible contributions of various factors, such as composition, porosity, microstructure (e.g., grain size and morphology), residual stress, and/or sample axis orientation relative to the additive manufacturing deposition trajectory, are considered to explain differences between the AM and baseline 304L dynamic material results.

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High Strain Rate Tensile Response of A572 and 4140 Steel

Procedia Engineering

Sanborn, Brett S.; Song, Bo S.; Thompson, Andrew D.; Reece, Blake D.; Attaway, Stephen W.

Steel grades such as A572 and AISI 4140 are often used for applications where high rate or impact loading may occur. A572 is a hot-rolled carbon steel that is used where a high strength to weight ratio is desired. A grade such as AISI 4140 offers decent corrosion resistance due to higher chromium and molybdenum content and is commonly used in firearm parts, pressurized gas tubes, and structural tubing for roll cages. In these scenarios, the material may undergo high rate loading. Thus, material properties including failure and fracture response at relevant loading rates must be understood so that numerical simulations of impact events accurately capture the deformation and failure/fracture behavior of the involved materials. In this study, the high strain rate tensile response of A572 and 4140 steel are investigated. An increase in yield strength of approximately 28% was observed for 4140 steel when comparing 0.001 s-1 strain rate to 3000 s-1 experiments. A572 showed an increase in yield strength of approximately 52% when the strain rate increased from quasi-static to 2750 s-1. Effects on true stress and strain at failure for the two materials are also discussed.

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Wave transmission through silicone foam pads in a compression Kolsky bar apparatus. Comparisons between simulations and measurements

Corona, Edmundo C.; Song, Bo S.

This memo concerns the transmission of mechanical signals through silicone foam pads in a compression Kolsky bar set-up. The results of numerical simulations for four levels of pad pre-compression and two striker velocities were compared directly to test measurements to assess the delity of the simulations. The nite element model simulated the Kolsky tests in their entirety and used the hyperelastic `hyperfoam' model for the silicone foam pads. Calibration of the hyperfoam model was deduced from quasi-static compression data. It was necessary, however, to augment the material model by adding sti ness proportional damping in order to generate results that resembled the experimental measurements. Based on the results presented here, it is important to account for the dynamic behavior of polymeric foams in numerical simulations that involve high loading rates.

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Dynamic Characterization and Stress-Strain Symmetry of Vascomax® C250 Maraging Steel in Compression and Tension

Procedia Engineering

Song, Bo S.; Sanborn, Brett S.; Wakeland, P.; Furnish, Michael D.

Low carbon, high strength steel alloys such as Vascomax steels are used in a wide variety of extreme environments due to their high strength, high fracture toughness, and stability over a wide range of temperatures. In this study, Vascomax® C250 steel was dynamically characterized in compression using Kolsky compression bar techniques at two strain rates of 1000 and 3000 s-1. A pair of impedance-matched tungsten carbide platens were implemented to protect damage to the bar ends. The tungsten carbide platens were experimentally calibrated as system compliance which was then properly corrected for actual specimen strain measurements. In addition, elastic indentation of the high-strength compression sample into the platens was also evaluated and showed negligible effect on the specimen strain measurements. The Vascomax® C250 steel exhibited strain-rate effects on the compressive stress-strain curves. The dynamic yield strength was approximately 18% higher than quasi-static yield strength obtained from hardness tests. The dynamic true stress-strain curves of the Vascomax® C250 steel in compression were also computed and then compared with the previously obtained true tensile stress-strain curves at the same strain rates. The Vascomax® C250 steel exhibited a reasonable symmetry in dynamic compression and tensile stress-strain response. However, the fracture strains in dynamic compression were smaller than those in dynamic tension probably due to different fracture mechanisms in the different loading modes.

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Pre-strain Effect on Frequency-Based Impact Energy Dissipation through a Silicone Foam Pad for Shock Mitigation

Journal of Dynamic Behavior of Materials

Sanborn, Brett S.; Song, Bo S.; Smith, Scott

Silicone foams have been used in a variety of applications from gaskets to cushioning pads over a wide range of environments. Particularly, silicone foams are used as a shock mitigation material for shock and vibration applications. Understanding the shock mitigation response, particularly in the frequency domain, is critical for optimal designs to protect internal devices and components more effectively and efficiently. The silicone foams may be subjected to pre-strains during the assembly process which may consequently influence the frequency response with respect to shock mitigation performance. A Kolsky compression bar was modified with pre-compression capabilities to characterize the shock mitigation response of silicone foam in the frequency domain to determine the effect of pre-strain. A silicone sample was also intentionally subjected to repeated pre-strain and dynamic loadings to explore the effect of repeated loading on the frequency response of shock mitigation.

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Highly stretchable miniature strain sensor for large strain measurement

Conference Proceedings of the Society for Experimental Mechanics Series

Yao, Shurong; Nie, Xu; Yu, Xun; Song, Bo S.; Blecke, Jill B.

In this research, a new type of highly stretchable strain sensor was developed to measure large strains. The sensor was based on the piezo-resistive response of carbon nanotube (CNT)/polydimethylsiloxane (PDMS) composite thin films. The piezo-resistive response of CNT composite gives accurate strain measurement with high frequency response, while the ultra-soft PDMS matrix provides high flexibility and ductility for large strain measurement. Experimental results show that the CNT/PDMS sensor measures large strains (up to 8 %) with an excellent linearity and a fast frequency response. The new miniature strain sensor also exhibits much higher sensitivities than the conventional foil strain gages, as its gauge factor is 500 times of that of the conventional foil strain gages.

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Dynamic compressive response of wrought and additive manufactured 304L stainless steels

EPJ Web of Conferences

Nishida, E.E.; Song, Bo S.; Maguire, Michael C.; Adams, David P.; Carroll, Jay D.; Wise, Jack L.; Bishop, Joseph E.; Palmer, Todd

Additive manufacturing (AM) technology has been developed to fabricate metal components that include complex prototype fabrication, small lot production, precision repair or feature addition, and tooling. However, the mechanical response of the AM materials is a concern to meet requirements for specific applications. Differences between AM materials as compared to wrought materials might be expected, due to possible differences in porosity (voids), grain size, and residual stress levels. When the AM materials are designed for impact applications, the dynamic mechanical properties in both compression and tension need to be fully characterized and understood for reliable designs. In this study, a 304L stainless steel was manufactured with AM technology. For comparison purposes, both the AM and wrought 304L stainless steels were dynamically characterized in compression Kolsky bar techniques. They dynamic compressive stress-strain curves were obtained and the strain rate effects were determined for both the AM and wrought 304L stainless steels. A comprehensive comparison of dynamic compressive response between the AM and wrought 304L stainless steels was performed. SAND2015-0993 C.

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Dynamic High-Temperature Tensile Characterization of an Iridium Alloy with Kolsky Tension Bar Techniques

Journal of Dynamic Behavior of Materials

Song, Bo S.; Nelson, Kevin N.; Lipinski, Ronald J.; Bignell, John B.; Ulrich, G.B.; George, E.P.

Conventional Kolsky tension bar techniques were modified to characterize an iridium alloy in tension at elevated strain rates and temperatures. The specimen was heated to elevated temperatures with an induction coil heater before dynamic loading; whereas, a cooling system was applied to keep the bars at room temperature during heating. A preload system was developed to generate a small pretension load in the bar system during heating in order to compensate for the effect of thermal expansion generated in the high-temperature tensile specimen. A laser system was applied to directly measure the displacements at both ends of the tensile specimen in order to calculate the strain in the specimen. A pair of high-sensitivity semiconductor strain gages was used to measure the weak transmitted force due to the low flow stress in the thin specimen at elevated temperatures. The dynamic high-temperature tensile stress–strain curves of a DOP-26 iridium alloy were experimentally obtained at two different strain rates (~1000 and 3000 s−1) and temperatures (~750 and 1030 °C). The effects of strain rate and temperature on the tensile stress–strain response of the iridium alloy were determined. The iridium alloy exhibited high ductility in stress–strain response that strongly depended on strain-rate and temperature.

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Dynamic high-temperature characterization of an iridium alloy in tension

Song, Bo S.; Nelson, Kevin N.; Jin, Huiqing J.; Lipinski, Ronald J.; Bignell, John B.; Ulrich, G.B.; George, E.P.

Iridium alloys have been utilized as structural materials for certain high-temperature applications, due to their superior strength and ductility at elevated temperatures. The mechanical properties, including failure response at high strain rates and elevated temperatures of the iridium alloys need to be characterized to better understand high-speed impacts at elevated temperatures. A DOP-26 iridium alloy has been dynamically characterized in compression at elevated temperatures with high-temperature Kolsky compression bar techniques. However, the dynamic high-temperature compression tests were not able to provide sufficient dynamic high-temperature failure information of the iridium alloy. In this study, we modified current room-temperature Kolsky tension bar techniques for obtaining dynamic tensile stress-strain curves of the DOP-26 iridium alloy at two different strain rates (~1000 and ~3000 s-1) and temperatures (~750°C and ~1030°C). The effects of strain rate and temperature on the tensile stress-strain response of the iridium alloy were determined. The DOP-26 iridium alloy exhibited high ductility in stress-strain response that strongly depended on both strain rate and temperature.

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Dynamic characterization of frequency response of shock mitigation of a polymethylene diisocyanate (PMDI) based rigid polyurethane foam

Latin American Journal of Solids and Structures

Song, Bo S.; Nelson, Kevin N.

Kolsky compression bar experiments were conducted to characterize the shock mitigation response of a polymethylene diisocyanate (PMDI) based rigid polyurethane foam, abbreviated as PMDI foam in this study. The Kolsky bar experimental data was analyzed in the frequency domain with respect to impact energy dissipation and acceleration attenuation to perform a shock mitigation assessment on the foam material. The PMDI foam material exhibits excellent performance in both energy dissipation and accele-ration attenuation, particularly for the impact frequency content over 1.5 kHz. This frequency (1.5 kHz) was observed to be independent of specimen thickness and impact speed, which may re-present the characteristic shock mitigation frequency of the PMDI foam material under investigation. The shock mitigation characteristics of the PMDI foam material were insignificantly influenced by the specimen thickness. However, impact speed did have some effect.

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Effect of twist on transverse impact response of ballistic fiber yarns

International Journal of Impact Engineering

Song, Bo S.; Lu, Wei-Yang L.

A Hopkinson bar was employed to conduct transverse impact testing of twisted Kevlar KM2 fiber yarns at the same impact speed. The speed of Euler transverse wave generated by the impact was measured utilizing a high speed digital camera. The study included fiber yarns twisted by different amounts. The Euler transverse wave speed was observed to increase with increasing amount of twist of the fiber yarn, within the range of this investigation. The higher transverse wave speeds in the more twisted fiber yarns indicate better ballistic performance in soft body armors for personal protection.

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Dynamic Tensile Characterization of Vascomax® Maraging C250 and C300 Alloys

Journal of Dynamic Behavior of Materials

Song, Bo S.; Wakeland, P.; Furnish, Michael D.

Vascomax® maraging C250 and C300 alloys were dynamically characterized in tension with Kolsky tension bar techniques. Compared with conventional Kolsky tension bar experiments, a pair of lock nuts was used to minimize the pseudo stress peak and a laser system was applied to directly measure the specimen displacement. Dynamic engineering stress–strain curves of the C250 and C300 alloys were obtained in tension at 1000 and 3000 s−1. The dynamic yield strengths for both alloys were similar, but significantly higher than those obtained from quasi-static indentation tests. Both alloys exhibited insignificant strain-rate effect on dynamic yield strength. The C300 alloy showed approximately 10 % higher in yield strength than the C250 alloy at the same strain rates. Necking was observed in both alloys right after yield. The Bridgman correction was applied to calculate the true stress and strain at failure for both alloys. The true failure stress showed a modest strain rate effect for both alloys but no significant difference between the two alloys at the same strain rate. The C250 alloy was more ductile than the C300 alloy under dynamic loading.

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A Novel Splitting-Beam Laser Extensometer Technique for Kolsky Tension Bar Experiment

Journal of Dynamic Behavior of Materials

Nie, Xu; Song, Bo S.; Loeffler, Colin M.

A modified laser occlusive extensometer technique was developed to measure the specimen strain with reasonably high and tunable resolutions in Kolsky tension bar experiments. This new technique used a novel concept where a laser beam was split into two independent sections to track the displacement histories of the incident and transmission bar ends, respectively, with independent resolutions. This technique ensures highly precise small strain measurements without sacrificing the capacity for large strain measurement. The uncertainty caused by rigid body motion of the specimen during dynamic strain measurement, which is induced by slight variation of laser intensity along the gage length, was also minimized in this technique. The validation test on Vascomax® maraging C250 alloy demonstrated that the new technique was capable of making both small and large strain measurements in Kolsky tension bar experiments, which is also applicable to Kolsky compression bar experiments.

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Effect of Threaded Joint Preparation on Impact Energy Dissipation Using Frequency-Based Kolsky Bar Analysis

Conference Proceedings of the Society for Experimental Mechanics Series

Werner, Brian T.; Song, Bo S.; Nelson, Kevin N.

Threaded joints are used in a wide range of industries and are relied upon in maintaining component assembly and structural integrity of mechanical systems. The threads may undergo specific preparation before assembly in applications. In order to ensure a tight seal the threads may be wrapped with PTFE tape or to prevent loosening over time an adhesive (thread locker) may be used. When a threaded joint is subjected to impact loading, the energy is transmitted through the joint to its neighbors while part of it is dissipated within the joint. In order to study the effect of the surface preparation to the threads, steel and aluminum joints were tested with no surface preparation, application of PTFE tape, and with the use of a thread locker (Loctite 262). The tests were conducted using a Kolsky tension bar and a frequency based analysis was used to characterize the energy dissipation of the various thread preparations on both steel/steel and steel/aluminum threaded joints. © The Society for Experimental Mechanics, Inc. 2015.

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Dynamic High-temperature Testing of an Iridium Alloy in Compression at High-strain Rates: Dynamic High-temperature Testing

Strain

Song, Bo S.; Nelson, Kevin N.; Lipinski, Ronald J.; Bignell, John B.

Iridium alloys are known to have superior strength and ductility at elevated temperatures, making them useful as structural materials for certain high-temperature applications. However, experimental data on their high-strain -rate performance are needed for understanding high-speed impacts in severe environments. Kolsky bars (also called split Hopkinson bars) have been extensively employed for high-strain -rate characterization of materials at room temperature, but it has been challenging to adapt them for the measurement of dynamic properties at high temperatures. In this study, we analyzed the difficulties encountered in high-temperature Kolsky bar testing of thin iridium alloy specimens in compression. Appropriate modifications were then made to the current high-temperature Kolsky bar technique to obtain reliable compressive stress–strain response of an iridium alloy at high-strain rates (300–10 000 s-1) and temperatures (750 and 1030 °C). Finally, the compressive stress–strain response of the iridium alloy showed significant sensitivity to both strain rate and temperature.

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Dynamic High-Temperature Characterization of an Iridium Alloy in Compression at High Strain Rates

Song, Bo S.; Nelson, Kevin N.; Lipinski, Ronald J.; Bignell, John B.; Ulrich, George U.; George, E.P.

Iridium alloys have superior strength and ductility at elevated temperatures, making them useful as structural materials for certain high-temperature applications. However, experimental data on their high-temperature high-strain-rate performance are needed for understanding high-speed impacts in severe elevated-temperature environments. Kolsky bars (also called split Hopkinson bars) have been extensively employed for high-strain-rate characterization of materials at room temperature, but it has been challenging to adapt them for the measurement of dynamic properties at high temperatures. Current high-temperature Kolsky compression bar techniques are not capable of obtaining satisfactory high-temperature high-strain-rate stress-strain response of thin iridium specimens investigated in this study. We analyzed the difficulties encountered in high-temperature Kolsky compression bar testing of thin iridium alloy specimens. Appropriate modifications were made to the current high-temperature Kolsky compression bar technique to obtain reliable compressive stress-strain response of an iridium alloy at high strain rates (300 – 10000 s-1) and temperatures (750°C and 1030°C). Uncertainties in such high-temperature high-strain-rate experiments on thin iridium specimens were also analyzed. The compressive stress-strain response of the iridium alloy showed significant sensitivity to strain rate and temperature.

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Dynamic Tensile Characterization of a 4330-V Steel with Kolsky Bar Techniques

Experimental Mechanics

Song, Bo S.; Antoun, Bonnie R.; Jin, H.

Dynamic tensile experimental techniques of high-strength alloys using a Kolsky tension bar implemented with pulse shaping and advanced analytical and diagnostic techniques have been developed. The issues that include minimizing abnormal stress peak, determining strain in specimen gage section, evaluating uniform deformation, as well as developing pulse shaping for constant strain rate and stress equilibrium have been addressed in this study to ensure valid experimental conditions and obtainment of reliable high-rate tensile stress-strain response of alloys with a Kolsky tension bar. The techniques were applied to characterize the tensile stress-strain response of a 4330-V steel at two high strain rates. Comparing these high-rate results with quasi-static data, the strain rate effect on the tensile stress-strain response of the 4330-V steel was determined. The 4330-V steel exhibits slight work-hardening behavior in tension and the tensile flow stress is significantly sensitive to strain rate. © 2013 Society for Experimental Mechanics.

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Development of high-temperature Kolsky compression bar techniques for recrystallization investigation

European Physical Journal: Special Topics

Song, Bo S.; Antoun, Bonnie R.; Song, Bo S.

We modified the design originally developed by Kuokkala's group to develop an automated high-temperature Kolsky compression bar for characterizing high-rate properties of 304L stainless steel at elevated temperatures. Additional features have been implemented to this high-temperature Kolsky compression bar for recrystallization investigation. The new features ensure a single loading on the specimen and precise time and temperature control for quenching to the specimen after dynamic loading. Dynamic compressive stress-strain curves of 304L stainless steel were obtained at 21, 204, 427, 649, and 871 °C (or 70, 400, 800, 1200, and 1600 °F) at the same constant strain rate of 332 s -1. The specimen subjected to specific time and temperature control for quenching after a single dynamic loading was preserved for investigating microstructure recrystallization. © 2012 EDP Sciences and Springer.

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High-speed transverse impact on a high performance ballistic fiber yarn

Song, Bo S.; Lu, Wei-Yang L.

Many ballistic fibers have been developed and utilized in soft body armors for military and law enforcement personnel. However, it is complex and challenging to evaluate the performance of ballistic resistance for the ballistic fibers. In applications, the fibers are subjected to high speed transverse impact by external objects. It is thus desirable to understand the dynamic response of the fibers under transverse impact. Transverse wave speed has been recognized a critical parameter for ballistic-resistant performance because a faster transverse wave speed dissipates the external impact energy more quickly. In this study, we employed split Hopkinson pressure bar (SHPB) and gas gun to conduct high-speed impact on a Kevlar fiber bundle in the transverse direction at different velocities. The deformation of the fiber bundle was photographed with high-speed digital cameras. Additional sensitive transducers were employed to provide more quantitative information of the fiber response during such a transverse impact. The experimental results were used for quantitative verification of current analytical models.

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Dynamic tensile characterization of a 4330-V steel with kolsky bar techniques

Song, Bo S.; Connelly, Kevin C.

There has been increasing demand to understand the stress-strain response as well as damage and failure mechanisms of materials under impact loading condition. Dynamic tensile characterization has been an efficient approach to acquire satisfactory information of mechanical properties including damage and failure of the materials under investigation. However, in order to obtain valid experimental data, reliable tensile experimental techniques at high strain rates are required. This includes not only precise experimental apparatus but also reliable experimental procedures and comprehensive data interpretation. Kolsky bar, originally developed by Kolsky in 1949 [1] for high-rate compressive characterization of materials, has been extended for dynamic tensile testing since 1960 [2]. In comparison to Kolsky compression bar, the experimental design of Kolsky tension bar has been much more diversified, particularly in producing high speed tensile pulses in the bars. Moreover, instead of directly sandwiching the cylindrical specimen between the bars in Kolsky bar compression bar experiments, the specimen must be firmly attached to the bar ends in Kolsky tensile bar experiments. A common method is to thread a dumbbell specimen into the ends of the incident and transmission bars. The relatively complicated striking and specimen gripping systems in Kolsky tension bar techniques often lead to disturbance in stress wave propagation in the bars, requiring appropriate interpretation of experimental data. In this study, we employed a modified Kolsky tension bar, newly developed at Sandia National Laboratories, Livermore, CA, to explore the dynamic tensile response of a 4330-V steel. The design of the new Kolsky tension bar has been presented at 2010 SEM Annual Conference [3]. Figures 1 and 2 show the actual photograph and schematic of the Kolsky tension bar, respectively. As shown in Fig. 2, the gun barrel is directly connected to the incident bar with a coupler. The cylindrical striker set inside the gun barrel is launched to impact on the end cap that is threaded into the open end of the gun barrel, producing a tension on the gun barrel and the incident bar.

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Stress wave propagation in a composite beam subjected to transverse impact

Song, Bo S.; Jin, Huiqing J.; Lu, Wei-Yang L.

Composite materials, particularly fiber reinforced plastic composites, have been extensively utilized in many military and industrial applications. As an important structural component in these applications, the composites are often subjected to external impact loading. It is desirable to understand the mechanical response of the composites under impact loading for performance evaluation in the applications. Even though many material models for the composites have been developed, experimental investigation is still needed to validate and verify the models. It is essential to investigate the intrinsic material response. However, it becomes more applicable to determine the structural response of composites, such as a composite beam. The composites are usually subjected to out-of-plane loading in applications. When a composite beam is subjected to a sudden transverse impact, two different kinds of stress waves, longitudinal and transverse waves, are generated and propagate in the beam. The longitudinal stress wave propagates through the thickness direction; whereas, the propagation of the transverse stress wave is in-plane directions. The longitudinal stress wave speed is usually considered as a material constant determined by the material density and Young's modulus, regardless of the loading rate. By contrast, the transverse wave speed is related to structural parameters. In ballistic mechanics, the transverse wave plays a key role to absorb external impact energy [1]. The faster the transverse wave speed, the more impact energy dissipated. Since the transverse wave speed is not a material constant, it is not possible to be calculated from stress-wave theory. One can place several transducers to track the transverse wave propagation. An alternative but more efficient method is to apply digital image correlation (DIC) to visualize the transverse wave propagation. In this study, we applied three-pointbending (TPB) technique to Kolsky compression bar to facilitate dynamic transverse loading on a glass fiber/epoxy composite beam. The high-speed DIC technique was employed to study the transverse wave propagation.

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Compressive behavior of fine sand

Song, Bo S.

The compressive mechanical response of fine sand is experimentally investigated. The strain rate, initial density, stress state, and moisture level are systematically varied. A Kolsky bar was modified to obtain uniaxial and triaxial compressive response at high strain rates. A controlled loading pulse allows the specimen to acquire stress equilibrium and constant strain-rates. The results show that the compressive response of the fine sand is not sensitive to strain rate under the loading conditions in this study, but significantly dependent on the moisture content, initial density and lateral confinement. Partially saturated sand is more compliant than dry sand. Similar trends were reported in the quasi-static regime for experiments conducted at comparable specimen conditions. The sand becomes stiffer as initial density and/or confinement pressure increases. The sand particle size become smaller after hydrostatic pressure and further smaller after dynamic axial loading.

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Size Effect in Continuum Modeling

Foulk, James W.; Connelly, Kevin C.; Song, Bo S.; Yang, Nancy Y.; Lu, Wei-Yang L.

The mechanical properties of some materials (Cu, Ni, Ag, etc.) have been shown to develop strong dependence on the geometric dimensions, resulting in a size effect. Several theories have been proposed to model size effects, but have been based on very few experiments conducted at appropriate scales. Some experimental results implied that size effects are caused by increasing strain gradients and have been used to confirm many strain gradient theories. On the other hand, some recent experiments show that a size effect exists in the absence of strain gradients. This report describes a brief analytical and experimental study trying to clarify the material and experimental issues surrounding the most influential size-effect experiments by Fleck et al (1994). This effort is to understand size effects intended to further develop predictive models.

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142 Results
142 Results